QCKTQG Doi Voi Cac San Pham Chat Beo Tu Sua

8/6/2019 QCKTQG Doi Voi Cac San Pham Chat Beo Tu Sua

1/18

QCVN 5-4:2010/BYT

QUY CHUN K THUT QUC GIA

I VI CC SN PHM CHT BO T SA

National technical regulation for dairy fat products

1. QUY NH CHUNG1.1. Phm vi iu chnh

Quy chun ny quy nh cc ch tiu an ton thc phm v cc yu cu qun

l i vi cc sn phm cht bo t sa, bao gm cc sn phm cream (ngoi tr

cream bt), b, du b, cht bo sa v cht bo t sa dng pht.

1.2. i tng p dng

Quy chun ny p dng i vi:a) Cc t chc, c nhn nhp khu, sn xut, kinh doanh cc sn phm cht

bo t sa ti Vit Nam;

b) Cc t chc, c nhn c lin quan.

1.3. Gii thch t ng

Trong Quy chun ny, cc t ng di y c hiu nh sau:

1.3.1. Cream dng lngL sn phm giu cht bo, dng nh tng thu c bng cch tch l hc

t sa.

1.3.2. B

L sn phm cht bo c ch bin t sa hoc sn phm sa, ch yu di

dng nh tng.

1.3.3. Cht bo sa (milkfat) v du b (butteroil); cht bo sa tchnc (anhydrous milkfat) v du b tch nc (anhydrous butteroil)

L sn phm cht bo c ngun gc t sa hoc sn phm sa, c ch

bin bng cc phng php sao cho tch c hu ht nc v cht kh khng

bo.

1.3.4. Cht bo t sa dng pht

L sn phm cht bo c ngun gc t sa, dng nh tng hoc dngmm c th pht c.

3


2/18

QCVN 5-4:2010/BYT

2. QUY NH V K THUT

2.1. Cc ch tiu lin quan n an ton thc phm i vi cc sn phm

cht bo t sa

2.1.1. Cc ch tiu l ho c quy nh ti Ph lc I ca Quy chun ny.

2.1.2. Gii hn ti a cc cht nhim bn c quy nh ti Ph lc II ca Quy

chun ny.

2.1.3. Cc ch tiu vi sinh vt c quy nh ti Ph lc III ca Quy chun

ny.

2.1.4. Danh mc ph gia thc phm c php s dng ph hp vi quy nh

hin hnh.

2.1.5. C th s dng cc phng php th c chnh xc tng ng vi

cc phng php quy nh km theo cc ch tiu trong cc Ph lc I, Ph lc II v

Ph lc III ca Quy chun ny.

2.1.6. S hiu v tn y ca phng php ly mu v cc phng php

th c quy nh ti Ph lc IV ca Quy chun ny.

2.1.7. Trong trng hp cn kim tra cc ch tiu cha quy nh phng php

th ti Quy chun ny, B Y t s quyt nh cn c theo cc phng php hin

hnh trong nc hoc ngoi nc c xc nhn gi tr s dng.

2.2. Ghi nhn Vic ghi nhn cc sn phm cht bo t sa phi theo ng

quy nh ti Ngh nh s 89/2006/N-CP ngy 30/8/2006 ca Chnh ph v nhn

hng ho v cc vn bn hng dn thi hnh.

3. QUY NH V QUN L

3.1. Cng b hp quy

3.1.1. Cc sn phm cht bo t sa c nhp khu, sn xut, kinh doanh trong

nc phi c cng b hp quy ph hp vi cc quy nh ti Quy chun ny.

3.1.2. Phng thc, trnh t, th tc cng b hp quy c thc hin theo

Quy nh v chng nhn hp chun, chng nhn hp quy v cng b hp chun,

4


3/18

QCVN 5-4:2010/BYT

cng b hp quy c ban hnh km theo Quyt nh s 24/2007/Q-BKHCN

ngy 28 thng 9 nm 2007 ca B trng B Khoa hc v Cng ngh v cc quy

nh ca php lut.

3.2. Kim tra i vi cc sn phm cht bo t saVic kim tra cht lng, v sinh an ton i vi cc sn phm cht bo t

sa phi c thc hin theo cc quy nh ca php lut.

4. TRCH NHIM CA T CHC, C NHN

4.1. T chc, c nhn nhp khu, sn xut cc sn phm cht bo t sa phi

cng b hp quy ph hp vi cc quy nh k thut ti Quy chun ny, ng kbn cng b hp quy ti c quan qun l nh nc c thm quyn theo phn cp

ca B Y t v bo m cht lng, v sinh an ton theo ng ni dung cng

b.

4.2. T chc, c nhn ch c nhp khu, sn xut, kinh doanh cc sn phm

cht bo t sa sau khi hon tt ng k bn cng b hp quy v bo m cht

lng, v sinh an ton, ghi nhn ph hp vi cc quy nh ca php lut.

5. T CHC THC HIN

5.1. Giao Cc An ton v sinh thc phm ch tr, phi hp vi cc c quan

chc nng c lin quan hng dn trin khai v t chc vic thc hin Quy chun

ny.

5.2. Cn c vo yu cu qun l, Cc An ton v sinh thc phm c trchnhim kin ngh B Y t sa i, b sung Quy chun ny.

5.3. Trong trng hp cc tiu chun v quy nh php lut c vin dn

trong Quy chun ny c s thay i, b sung hoc c thay th th p dng theo

vn bn mi.

5


4/18

QCVN 5-4:2010/BYT

Ph lc I

CC CH TIU L HO CA CC SN PHM CHT BO T SA

Tn ch tiu Mc quynh

Phng phpth Phn loich tiu 1)

I. Cream dng lng

1. Hm lng cht bo sa, % khilng, khng nh hn

10 ISO 2450:1999 A

II. B

1. m, % khi lng, khng lnhn

16 TCVN 8151-1:2009 (ISO3727-1:2001)

A


80 TCVN 8151-3:2009 (ISO

3727-3:2003);TCVN 8154:2009(ISO 17189:2003)

B

3. Ch s peroxyd, mili ng lng

oxy hot ng/kg cht bo

0,3 ISO 3976:2006 A

III. Cht bo sa (milkfat) v du b (butter oil)


99,6 TCVN 8154:2009(ISO 17189:2003)

A

2. Ch s peroxyd, mili ng lngoxy hot ng/kg cht bo

0,6 ISO 3976:2006 A

IV. Cht bo sa tch nc (anhydrous milkfat) v du b tch nc(anhydrous butter oil)

1. Hm lng nc, % khi lng,khng ln hn

0,1 TCVN 7728:2007(ISO 5536:2002)

A


99,8 TCVN 8154:2009(ISO 17189:2003)

A

3. Ch s peroxyd, mili ng lngoxy hot ng/kg cht bo

0,3 ISO 3976:2006 A

V. Cht bo t sa dng pht

1. Hm lng cht bo sa, % khilng

t 10 ndi 80

TCVN 8154:2009(ISO 17189:2003)

A

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5/18

QCVN 5-4:2010/BYT

Tn ch tiu Mc quynh

Phng php

th

Phn loich tiu 1)

1) Ch tiu loi A: bt buc phi th nghim nh gi hp quy. Ch tiu loi B:khng bt buc phi th nghim nh gi hp quy nhng t chc, c nhn

sn xut, nh p khu, ch bin cc sn phm sa dng lng phi p ng cc yucu i vi ch tiu loi B.

7


6/18

QCVN 5-4:2010/BYT

Ph lc II

GII HN CC CHT NHIM BN

I VI CREAM V CC SN PHM CHT BO T SA

Tn ch tiu Giihn ti

a

Phng php th Phn loich tiu 2)

I. Kim loi nng1. Ch, mg/kg 0,02 TCVN 7933:2008

(ISO 6733:2006),

TCVN 7929:2008(EN 14083:2003)

A

2. Thic (i vi sn phm ngtrong bao b trng thic), mg/kg

250 TCVN 7730:2007(ISO/TS 9941:2005),

TCVN 8110:2009(ISO 14377:2002),TCVN 7788:2007

A

3. Antimony, mg/kg 1,0 TCVN 8132:2009 B4. Arsen, mg/kg 0,5 TCVN 7601:2007 B5. Cadmi, mg/kg 1,0 TCVN 7603:2007,

TCVN 7929:2008(EN 14083:2003)

B

6. Thu ngn, mg/kg 0,05 TCVN 7993:2008(EN 13806:2002)

B

II. c t vi nm1. Aflatoxin M1, g/kg 0,5 TCVN 6685:2009

(ISO 14501:2007)A

III. Melamin1. Melamin, mg/kg 2,5 Thng quy k thut

nh lng melamintrong thc phm

(Q 4143/Q-BYT)

B

IV. D lng thuc th y, g/kg1. Benzylpenicilin/Procain

benzylpenicilin4 TCVN 8106:2009

(ISO/TS

26844:2006);AOAC 988.08

A

8
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7/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


2. Clortetracyclin/Oxytetracyclin/Tetracyclin

100 TCVN 8106:2009(ISO/TS

26844:2006); AOAC995.04

A

3. Dihydrostreptomycin/Streptomycin

200 TCVN 8106:2009(ISO/TS

26844:2006); AOAC988.08;

A

4. Gentamicin 200 TCVN 8106:2009(ISO/TS

26844:2006)

A

5. Spiramycin 200 TCVN 8106:2009(ISO/TS

26844:2006)

A

6. Ceftiofur 100 TCVN 8106:2009(ISO/TS

26844:2006)

B

7. Clenbuterol 50 B8. Cyfluthrin 3) 40 TCVN 8101:2009

(ISO 8260:2008)B

9. Cyhalothrin 3) 30 AOAC 998.01 B10. Cypermethrin v alpha-

cypermethrin100 US FDA PAM, Vol.

I, Section 304,E4/C2, C4;

TCVN 8101:2009(ISO 8260:2008)

B

11. Deltamethrin 3) 30 TCVN 8101:2009(ISO 8260:2008)

B

12. Diminazen 150 B13. Doramectin 15 B14. Eprinomectin 20 B15. Febantel/ Fenbendazol/

Oxfendazol100 B

16. Imidocarb 50 B

17. Isometamidium 100 B18. Ivermectin 10 B19. Lincomycin 150 AOAC 988.08 B

9


8/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


20. Neomycin 1500 TCVN 8106:2009(ISO/TS

26844:2006)

B

21. Pirlimycin 200 B22. Spectinomycin 200 B23. Sulfadimidin 25 AOAC 992.21 B24. Thiabendazol 3) 100 B25. Triclorfon (Metrifonat) 3) 50 B

V. D lng thuc bo v thc vt 4), mg/kgV.1. i vi thuc bo v thc vt tan trong nc hoc tan mt phn trong cht

bo1. Endosulfan 0,01 TCVN 7082:2002(ISO 3890:2000),

phn 1 v phn 2;TCVN 8170:2009(EN 1528:1996),phn 1, 2, 3 v 4

A

2. 2,4-D 0,01 US FDA PAM, Vol.

I, Section 402, E1

B

3. Abamectin 0,005 B4. Acephat 0,02 AOAC 970.52 B5. Aldicarb 0,01 US FDA PAM, Vol.

I, Section 401,E1+DL1

B

6. Aminopyralid 0,02 B7. Amitraz 0,01 B8. Bentazon 0,05 B9. Bifenazat 0,01 B10. Bifenthrin 0,05 AOAC 970.52 B11. Bitertanol 0,05 B12. Carbaryl 0,05 AOAC 964.18;

US FDA PAM, Vol.I, Section 401,

E1+DL1

B

13. Carbendazim 0,05 B

14. Carbofuran 0,05 US FDA PAM, Vol.I, Section 401, E1,

B

10


9/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


DL115. Carbosulfan 0,03 B16. Clormequat 0,5 B17. Clorpropham 0,0005 US FDA PAM, Vol.

I, Section 304, E4,C1-C4

B

18. Clorpyrifos 0,02 TCVN 8101:2009(ISO 8260:2008)

B

19. Clorpyrifos-methyl 0,01 TCVN 8101:2009(ISO 8260:2008)

B

20. Clethodim 0,05 B21. Clofentezin 0,05 B22. Cyhexatin 0,05 B23. Cyprodinil 0,0004 B24. Cyromazin 0,01 B25. Diclorvos 0,02 TCVN 8101:2009

(ISO 8260:2008)B

26. Difenoconazol 0,005 B27. Dimethenamid-p 0,01 B

28. Dimethipin 0,01 B29. Dimethoat 0,05 AOAC 970.52 B30. Dimethomorph 0,01 B31. Diquat 0,01 B32. Disulfoton 0,01 B33. Dithiocarbamat 0,05 B34. Ethephon 0,05 B35. Ethoprophos 0,01 US FDA PAM, Vol.

I, Section 304, E4,C1, C3

B

36. Fenamiphos 0,005 B37. Fenbuconazol 0,05 B38. Fenbutatin oxid 0,05 B39. Fenpropimorph 0,01 B40. Fipronil 0,02 US FDA PAM, Vol.


B

41. Fludioxonil 0,01 B42. Flutolanil 0,05 B43. Glufosinat-amoni 0,02 B

11
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10/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


44. Imidacloprid 0,02 B45. Indoxacarb 0,1 B46. Kresoxim-methyl 0,01 B47. Lindan 0,01 AOAC 970.52 B48. Methamidophos 0,02 B49. Methidathion 0,001 US FDA PAM, Vol.


B

50. Methomyl 0,02 US FDA PAM, Vol.I, Section 401, E1,

DL1

B

51. Methoxyfenozid 0,01 B52. Myclobutanil 0,01 B53. Novaluron 0,4 B54. Oxamyl 0,02 US FDA PAM, Vol.

I, Section 401, E1,DL1

B

55. Oxydemeton-methyl 0,01 B56. Paraquat 0,005 B57. Penconazol 0,01 B58. Pirimicarb 0,01 B59. Pirimiphos-methyl 0,01 TCVN 8101:2009

(ISO 8260:2008)B

60. Procloraz 0,05 B61. Profenofos 0,01 US FDA PAM, Vol.


B

62. Propamocarb 0,01 B63. Propiconazol 0,01 B64. Pyraclostrobin 0,03 B65. Pyrimethanil 0,01 US FDA PAM, Vol.


B

66. Quinoxyfen 0,01 B67. Spinosad 1 B68. Tebuconazol 0,01 B69. Tebufenozid 0,01 B70. Terbufos 0,01 US FDA PAM, Vol. B

12


11/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


I, Section 304, C1-C4

71. Thiacloprid 0,05 B72. Triadimefon 0,01 US FDA PAM, Vol.

I, Section 304, C1,C3

B

73. Triadimenol 0,01 B74. Trifloxystrobin 0,02 B75. Vinclozolin 0,05 US FDA PAM, Vol.

I, Section 304, C1-

C3; E1-E5+C6

B

V.2. i vi thuc bo v thc vt tan trong cht bo 5)

1. Aldrin v dieldrin 0,006 TCVN 7082:2002(ISO 3890:2000),

phn 1 v phn 2;TCVN 8101:2009(ISO 8260:2008);TCVN 8170:2009

(EN 1528:1996),phn 1, 2, 3 v 4

A

2. Cyfluthrin 6) 0,04 TCVN 8101:2009(ISO 8260:2008)

A

3. Clordan 0,002 TCVN 7082:2002(ISO 3890:2000),

phn 1 v phn 2;TCVN 8170:2009

(EN 1528:1996),phn 1, 2, 3 v 4

B

4. Cypermethrin 0,05 US FDA PAM, Vol.I, Section 304,

E4/C2, C4;TCVN 8101:2009(ISO 8260:2008)

B

5. DDT 0,02 TCVN 7082:2002

(ISO 3890:2000),phn 1 v phn 2;

A

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12/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


TCVN 8170:2009(EN 1528:1996),phn 1, 2, 3 v 4

6. Deltamethrin 6) 0,05 TCVN 8101:2009(ISO 8260:2008)

B

7. Diazinon 0,02 TCVN 8101:2009(ISO 8260:2008)

B

8. Dicofol 0,1 TCVN 8101:2009(ISO 8260:2008)

B

9. Diflubenzuron 0,02 B

10. Diphenylamin 0,0004 B11. Famoxadin 0,03 B12. Fenhexamid 0,01 B13. Fenpropathrin 0,1 US FDA PAM Vol.


B

14. Fenpyroximat 0,005 B15. Fenvalerat 0,1 TCVN 8101:2009

(ISO 8260:2008);AOAC 998.01

B

16. Flumethrin 0,05 B17. Flusilazol 0,05 B18. Heptaclor 0,006 TCVN 7082:2002

(ISO 3890:2000),phn 1 v phn 2;TCVN 8170:2009

(EN 1528:1996),phn 1, 2, 3 v 4

B

19. Methopren 0,1 B20. Permethrin 0,1 TCVN 8101:2009

(ISO 8260:2008)B

21. Phorat 0,01 US FDA PAM Vol.I, Section 304, C2,

C4

B

22. Piperonyl butoxid 0,05 US FDA PAM Vol.

I, Section 401, E1,DL2

B

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13/18

QCVN 5-4:2010/BYT

Tn ch tiu Giihn ti

a


23. Propargit 0,1 US FDA PAM Vol.I, Section 304,

E4+C6

B

2) Chi tiu loai A: bt buc phi th nghim nh gi hp quy. Ch tiu loi

B: khng bt buc phi th nghim nh gi hp quy nhng t chc, c nhn

sn xut, nhp khu, ch bin cc sn phm sa dng lng phi p ng cc yu

cu i vi ch tiu loi B.

3) Cng c dng lm thuc bo v thc vt.

4) Tham kho cc phng php th trong TCVN 5142:2008 (CODEX STAN 229-

1993, Rev.1-2003) Phn tch d lng thuc bo v thc vt Cc phng php

khuyn co.

5) Gii hn ny quy nh cho sn phm sa thanh trng v sa tit trng. i vi

cream v cc sn phm cht bo t sa, p dng mc gii hn bng 25 ln quy nh

ny, tnh trn c s cht bo trong sn phm sa.6) Cng c dng lm thuc th y.

15


14/18

QCVN 5-4:2010/BYT

Ph lc III

CC CH TIU VI SINH VT CA CC SN PHM CHT BO T SA

Tn ch tiu K hochly mu Gii hn Phng php th Phnloi ch

tiu 11)n7) c 8) m 9) M 10)

I. Cream v b1. E. coli 5 2 10

CFU/g

100

CFU/g

TCVN 7924-1:2008

(ISO 16649-

1:2001); TCVN

7924-2:2008 (ISO

16649-2:2001)

A

2.L. monocytogenes

(i vi sn phm

dng ngay)

5 0 100CFU/g TCVN 7700-

2:2007 (ISO

11290-2:1998,

With amd.1:2004)

A

3. Salmonella 5 0 Khng pht

hin trong 25 g

TCVN 4829:2005

(ISO 6579:2002,

With amd.1:2004)

A

II. Cht bo sa (milkfat) v du b (butteroil); cht bo sa tch nc

(anhydrous milkfat) v du b tch nc (anhydrous butteroil) v cht bo

t sa dng phtL. monocytogenes (i

vi sn phm dng

ngay)

5 0 100CFU/g TCVN 7700-

2:2007 (ISO

11290-2:1998,

With amd.1:2004)

A

7)

n: s n v mu c ly t l hng cn kim tra.8) c: s n v mu ti a c th chp nhn hoc s n v mu ti a cho phpvt qu ch tiu vi sinh vt m. Nu vt qu s n v mu ny th l hng ccoi l khng t.9) m: s lng hoc mc ti a vi khun c trong 1 gam sn phm; cc gi tr vtqu mc ny th c th c chp nhn hoc khng c chp nhn.10) M: l mc vi sinh vt ti a c dng phn nh gia cht lng sn phmc th t v khng t.11) Ch tiu loi A: bt buc phi th nghim nh gi hp quy.

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QCVN 5-4:2010/BYT

Ph lc IV

DANH MC PHNG PHP TH CC CH TIU AN TON THC

PHM I VI CC SN PHM CHT BO T SA

I. Ly mu1. TCVN 6400 (ISO 707) Sa v sn phm sa Hng dn ly mu.

II. Phng php th cc ch tiu l ho1. ISO 2450:1999 Cream Determination of fat content Gravimetric method

(Reference method) [Cream Xc nh hm lng cht bo Phng php

khi lng (Phng php chun)]2. ISO 3976:2006 Milk fat Determination of peroxide value (Cht bo sa

Xc nh ch s peroxit)3. TCVN 7728:2007 (ISO 5536:2002) Sn phm cht bo sa Xc nh hm

lng nc Phng php Karl Fischer4. TCVN 8151-1:2009 (ISO 3727-1:2001) B Xc nh m, hm lng

cht kh khng bo v hm lng cht bo Phn 1: Xc nh m

(Phng php chun)5.

TCVN 8151-3:2009 (ISO 3727-3:2003) B Xc nh m, hm lngcht kh khng bo v hm lng cht bo Phn 3: Tnh hm lng cht

bo6. TCVN 8154:2009 (ISO 17189:2003) B, nh tng du thc phm v cht

bo dng pht Xc nh hm lng cht bo (Phng php chun)

III. Phng php th cc cht nhim bn

III.1. Kim loi nng1. TCVN 6270:1997 (ISO 6732:1985) Sa v cc sn phm sa Xc nh

hm lng st Phng php quang ph (Phng php chun)2. TCVN 6352:1998 (ISO 8294:1998) Du, m ng vt v thc vt - Xc

nh hm lng ng, st, niken Phng php quang ph hp th nguyn

t dng l graphit3. TCVN 6353:2007 (ISO 12193:2004) Du m ng vt v thc vt Xc

nh ch bng phng php quang ph hp th nguyn t trc tip dng l

graphit4. TCVN 6354:1998 Du, m ng vt v thc vt Xc nh asen bng

17
http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=26546&ICS1=67&ICS2=100&ICS3=99http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=38685&ICS1=67&ICS2=100&ICS3=10http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=35212&ICS1=67&ICS2=100&ICS3=20http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=29475&ICS1=67&ICS2=100&ICS3=20http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=32902&ICS1=67&ICS2=100&ICS3=20http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=26546&ICS1=67&ICS2=100&ICS3=99http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=38685&ICS1=67&ICS2=100&ICS3=10http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=35212&ICS1=67&ICS2=100&ICS3=20http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=29475&ICS1=67&ICS2=100&ICS3=20http://www.iso.org/iso/iso_catalogue/catalogue_ics/catalogue_detail_ics.htm?csnumber=32902&ICS1=67&ICS2=100&ICS3=20


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QCVN 5-4:2010/BYT

phng php dng bc dietyldithiocacbamat5. TCVN 7601:2007 Thc phm Xc nh hm lng asen bng phng

php bc dietyldithiocacbamat6. TCVN 7603:2007 Thc phm Xc nh hm lng cadimi bng phng

php quang ph hp th nguyn t7. TCVN 7730:2007 (ISO/TS 9941:2005) Sa v sa c c ng hp Xc

nh hm lng thic Phng php o ph8. TCVN 7788:2007 hp thc phm Xc nh hm lng thic bng

phng php quang ph hp th nguyn t9. TCVN 7929:2008 (EN 14083:2003) Thc phm Xc nh cc nguyn t

vt Xc nh ch, cadimi, crom, molypden bng o ph hp th nguyn t

dng l graphit (GFAAS) sau khi phn hu bng p lc

10.TCVN 7933:2008 (ISO 6733:2006) Sa v sn phm sa Xc nh hmlng ch Phng php quang ph hp th nguyn t dng l graphit

11. TCVN 7993:2008 (EN 13806:2002) Thc phm Xc nh cc nguyn t

vt Xc nh thu ngn bng o ph hp th nguyn t hi-lnh (CVAAS)

sau khi phn hu bng p lc

III.2. c t vi nm1. TCVN 6685:2009 (ISO 14501:2007) Sa v sa bt Xc nh hm lng

aflatoxin M1 Lm sch bng sc k i lc min dch v xc nh bng sck lng hiu nng cao

III.3. Melamin1. Thng quy k thut nh lng melamin trong thc phm, c c ban

hnh km theo Quyt nh s 4143/Q-BYT ngy 22 thng 10 nm 2008

III.4. D lng thuc th y1. TCVN 8101:2009 (ISO 8260:2008) Sa v sn phm sa Xc nh thuc

bo v thc vt nhm clo hu c v polyclo biphenyl Phng php sc k

kh-lng mao qun c detector bt gi electron2. TCVN 8106:2009 (ISO/TS 26844:2006) Sa v sn phm sa Xc nh d

lng khng sinh Php th phn tn trong ng nghim3. AOAC 988.08 Antimicrobial Drugs in Milk. Microbial Receptor Assay

(Thuc khng sinh trong sa)4. AOAC 992.21 Sulfamethazine Residues in Raw Bovine Milk (D lng

sulfamethazine trong sa b ti)5. AOAC 995.04 Multiple Tetracycline Residues in Milk. Metal Chelate

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QCVN 5-4:2010/BYT

Affinity-Liquid Chromatographic Method (D lng tetracycline trong sa.

Phng php i lc chelat kim loi-sc k lng6. AOAC 995.09 Chlortetracycline, Oxytetracycline, and Tetracycline in

Edible Animal Tissues. Liquid Chromatographic Method (Chlortetracycline,

oxytetracycline v tetracycline trong tht ng vt. Phng php sc k lng)7. AOAC 998.01 Synthetic Pyrethroids in Agricultural Products Multiresidue.

GC Method (Pyrethroid tng hp trong nng sn. Phng php sc k kh)8. Pesticide Analytical Manual (PAM), Food and Drug Administration,

Washington, D.C., USA, Vol. I, 3rd edition, Section 3049. Pesticide Analytical Manual (PAM), Food and Drug Administration,

Washington, D.C., USA, Vol. I, 3rd edition, Section 40110. Pesticide Analytical Manual (PAM), Food and Drug Administration,

Washington, D.C., USA, Vol. I, 3rd edition, Section 402

III.5. D lng thuc bo v thc vt1. TCVN 5142:2008 (CODEX STAN 229-1993, Rev.1-2003) Phn tch d

lng thuc bo v thc vt Cc phng php khuyn co2. TCVN 7082-1:2002 (ISO 3890-1:2000) Sa v sn phm sa Xc nh d

lng hp cht clo hu c (thuc tr su) Phn 1: Xem xt chung v

phng php chit

3. TCVN 7082-2:2002 (ISO 3890-2:2000) Sa v sn phm sa Xc nh dlng hp cht clo hu c (thuc tr su) Phn 2: Phng php lm sch

dch chit th v th khng nh4. TCVN 8101:2009 (ISO 8260:2008) Sa v sn phm sa Xc nh thuc

bo v thc vt nhm clo hu c v polyclo biphenyl Phng php sc k

kh-lng mao qun c detector bt gi electron5. TCVN 8170-1:2009 (EN 1528-1:1996) Thc phm cha cht bo Xc nh

thuc bo v thc vt v polyclo biphenyl (PCB) Phn 1: Yu cu chung6. TCVN 8170-2:2009 (EN 1528-2:1996) Thc phm cha cht bo Xc nh

thuc bo v thc vt v polyclo biphenyl (PCB) Phn 2: Chit cht bo,

thuc bo v thc vt, PCB v xc nh hm lng cht bo7. TCVN 8170-3:2009 (EN 1528-3:1996) Thc phm cha cht bo Xc nh

thuc bo v thc vt v polyclo biphenyl (PCB) Phn 3: Cc phng php

lm sch8. TCVN 8170-4:2009 (EN 1528-4:1996) Thc phm cha cht bo Xc nh

thuc bo v thc vt v polyclo biphenyl (PCB) Phn 4: Xc nh, khng

nh, cc qui trnh khc

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QCVN 5-4:2010/BYT

9. AOAC 964.18 Carbaryl Pesticide Residues. Colorimetric Method (D lng

thuc bo v thc vt carbaryl. Phng php o mu)10. AOAC 970.52 Organochlorine and Organophosphorus Pesticide Residues.

General Multiresidue Method (D lng thuc bo v thc vt clo hu c v

phospho hu c. Phng php a d lng)

IV. Phng php th cc ch tiu vi sinh vt1. TCVN 4829:2005 (ISO 6579:2002, With amd.1:2004) Vi sinh vt trong

thc phm v thc n chn nui Phng php pht hin Salmonella trn

a thch2. TCVN 7700-2:2007 (ISO 11290-2:1998, With amd.1:2004) Vi sinh vt trong

thc phm v thc n chn nui Phng php pht hin v nh lng

Listeria monocytogenes Phn 2: Phng php nh lng3. TCVN 7924-1:2008 (ISO 16649-1:2001) Vi sinh vt trong thc phm v

thc n chn nui Phng php nh lngEscherichia coli dng tnh

-glucuronidaza Phn 1: K thut m khun lc 44 oC s dng mng

lc v 5-bromo-4-clo-3-indolyl -D-glucuronid4. TCVN 7924-2:2008 (ISO 16649-2:2001) Vi sinh vt trong thc phm v

thc n chn nui Phng php nh lngEscherichia coli dng tnh

-glucuronidaza Phn 2: K thut m khun lc 44 oC s dng 5-

bromo-4-clo-3-indolyl -D-glucuronid

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