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Carlos V. Opelt, Geraldo M. Cândido and Mirabel C. Rezende COMPRESSION FAILURE MODES OF CARBON FIBER FABRIC SCRAPS - EPOXY LAMINATES Technological Institute of Aeronautics São José dos Campos - Brazil Federal University of São Paulo São José dos Campos - Brazil

Normas ASTM Tribologia e Microdureza

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Page 1: Normas ASTM Tribologia e Microdureza

Carlos V. Opelt, Geraldo M. Cândido and Mirabel C. Rezende

COMPRESSION FAILURE MODES OF CARBON FIBER FABRIC SCRAPS - EPOXY LAMINATES

Technological Institute of Aeronautics

São José dos Campos - Brazil

Federal University of São Paulo

São José dos Campos - Brazil

Page 2: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 3: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 4: Normas ASTM Tribologia e Microdureza

• Few decades ago, the fiber reinforced polymer composites were considered the panacea of the materials for structural application.

• Over the years researchers have demonstrated that these materials are strongly affected by manufacturing defects and operation damages.

• The proper use of polymer composites requires the knowledge of their mechanical response under different loadings, as well as their failure mechanisms.

03 INTRODUCTION

Page 5: Normas ASTM Tribologia e Microdureza

• The compression behavior is a limiting in the design of structures made of carbon fiber reinforced polymers.

• The compressive strength of unidirectional carbon fiber/epoxy laminates is often less than 60% of their tensile strength.

• This relatively low compressive strength of polymer composites, compared to its tensile strength, is due to matrix properties governing the compressive failure.

04 INTRODUCTION

Page 6: Normas ASTM Tribologia e Microdureza

• The fiber-reinforced composites subjected to compressive loads can exhibit different failure modes with a different sequence of events to the fracture.

• There is a lack of consensus on the description and classification of the compressive failure modes that makes its assessment unfeasible.

• In some cases different authors end up describing the failure differently, despite the fracture aspects being very similar.

05 INTRODUCTION

Page 7: Normas ASTM Tribologia e Microdureza

• One example of classification is the one by ASTM standards (D3410M-03 e D6641-09).

06 INTRODUCTION

Page 8: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 9: Normas ASTM Tribologia e Microdureza

• Propose a classification that considers the failure modes already described in the literature and that can easily include new cases being reported.

• To present case studies that demonstrate how to apply this classification.

• Explore how the knowledge of the failure modes can help in the analysis and design of composite structures.

07 GOALS

Page 10: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 11: Normas ASTM Tribologia e Microdureza

• The proposed classification was based on the failure modes already reported in the literature, trying to cluster the ones with similar characteristics.

08 FAILURE MODES

Page 12: Normas ASTM Tribologia e Microdureza

• The proposed classification was based on the failure modes already reported in the literature, trying to cluster the ones with similar characteristics.

08 FAILURE MODES

Page 13: Normas ASTM Tribologia e Microdureza

In-plane Shear Through-the-thickness

Shear Wedge Splitting

09 SHEAR FAILURES

Page 14: Normas ASTM Tribologia e Microdureza

In-plane Shear

09 SHEAR FAILURES

Propagation in the width direction

Angled propagation

Page 15: Normas ASTM Tribologia e Microdureza

Through-the-thickness Shear

09 SHEAR FAILURES

Propagation in the thickness direction

Angled propagation

Flexural damages due to the sliding

surfaces

Page 16: Normas ASTM Tribologia e Microdureza

Wedge Splitting

09 SHEAR FAILURES

Two cracks propagating in the thickness direction

Formation of a wedge

Propagation of a large delamination

Page 17: Normas ASTM Tribologia e Microdureza

• The proposed classification was based on the failure modes already reported in the literature, trying to cluster the ones with similar characteristics.

08 FAILURE MODES

Page 18: Normas ASTM Tribologia e Microdureza

10 INTERLAMINAR FAILURES

Delamination Buckling Splitting

Page 19: Normas ASTM Tribologia e Microdureza

10 INTERLAMINAR FAILURES

Delamination Buckling

Buckling of the layers

Multiple delaminations

Splaying of the layers

Page 20: Normas ASTM Tribologia e Microdureza

10 INTERLAMINAR FAILURES

Splitting

Crushing of the layers

Multiple delaminations

Page 21: Normas ASTM Tribologia e Microdureza

• The proposed classification was based on the failure modes already reported in the literature, trying to cluster the ones with similar characteristics.

08 FAILURE MODES

Page 22: Normas ASTM Tribologia e Microdureza

11 INTERFACIAL FAILURES

Brooming Fiber Crushing

Page 23: Normas ASTM Tribologia e Microdureza

11 INTERFACIAL FAILURES

Brooming

Buckling of the fibers

Broom-like fracture

Extensive propagation of the interfacial cracks

Page 24: Normas ASTM Tribologia e Microdureza

11 INTERFACIAL FAILURES

Fiber Crushing

Restricted propagation of the interfacial cracks

Fibers are crushed against each other

Page 25: Normas ASTM Tribologia e Microdureza

• The proposed classification was based on the failure modes already reported in the literature, trying to cluster the ones with similar characteristics.

08 FAILURE MODES

Page 26: Normas ASTM Tribologia e Microdureza

12 KINK-BAND FAILURES

In-plane Kink-band Through-the-thickness

Shear

Page 27: Normas ASTM Tribologia e Microdureza

12 KINK-BAND FAILURES

In-plane Kink-band Propagation in the

width direction

Propagation of an angled band

The interfacial cracks are restricted to the band

Page 28: Normas ASTM Tribologia e Microdureza

12 KINK-BAND FAILURES

Through-the-thickness Shear

Propagation in the thickness direction

Propagation of an angled band

The interfacial cracks are restricted to the band

Page 29: Normas ASTM Tribologia e Microdureza

13 IRREGULAR PROPAGATION

Multiple Failure Modes Mixed Failure Modes

Page 30: Normas ASTM Tribologia e Microdureza

13 IRREGULAR PROPAGATION

Multiple Failure Modes

Irregular propagation in the width direction

Different failure modes in the two sides of the specimen

Page 31: Normas ASTM Tribologia e Microdureza

13 IRREGULAR PROPAGATION

Mixed Failure Modes

Irregular propagation in the width direction

Different failure modes in the two sides of the specimen

Page 32: Normas ASTM Tribologia e Microdureza

14 GLOBAL AND LOCAL MODES

Global Failure Mode Local Failure Mode

Page 33: Normas ASTM Tribologia e Microdureza

14 GLOBAL AND LOCAL MODES

Global Failure Mode Local Failure Mode

Fiber Crushing Failure

Wedge Splitting Failure

Page 34: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 35: Normas ASTM Tribologia e Microdureza

• J.M.F. Paiva; S. Mayer; M.C. Rezende "Evaluation of mechanical properties of four different carbon/epoxy composites used in aeronautical field" Materials Research (2005, vol. 8, p. 91).

• Carbon fibers arranged as a plain weave fabric.

• Prepreg (epoxy matrix) - HexPly® F155, Hexcel Composites

15 FABRIC LAMINATE

Page 36: Normas ASTM Tribologia e Microdureza

16 FABRIC LAMINATE

Page 37: Normas ASTM Tribologia e Microdureza

16 FABRIC LAMINATE

Angled propagation

Shear Failure

Page 38: Normas ASTM Tribologia e Microdureza

16 FABRIC LAMINATE

Debris from the sliding of the fracture surfaces

Shear Failure

Page 39: Normas ASTM Tribologia e Microdureza

17 FABRIC LAMINATE

Page 40: Normas ASTM Tribologia e Microdureza

17 FABRIC LAMINATE

Irregular propagation in the thickness direction

Mixed Failure Mode Shear Failure

+ Delamination Buckling

Page 41: Normas ASTM Tribologia e Microdureza

17 FABRIC LAMINATE

Angled propagation

Mixed Failure Mode Shear Failure

+ Delamination Buckling

Page 42: Normas ASTM Tribologia e Microdureza

17 FABRIC LAMINATE

Multiple delaminations

Mixed Failure Mode Shear Failure

+ Delamination Buckling

Page 43: Normas ASTM Tribologia e Microdureza

17 FABRIC LAMINATE

Splaying of the layers

Mixed Failure Mode Shear Failure

+ Delamination Buckling

Page 44: Normas ASTM Tribologia e Microdureza

18 FABRIC LAMINATE

Page 45: Normas ASTM Tribologia e Microdureza

18 FABRIC LAMINATE

Multiple Failure Modes Shear Failure Mode

+ Mixed Failure Modes

Page 46: Normas ASTM Tribologia e Microdureza

19 FABRIC LAMINATE

Local Failure Mode

Page 47: Normas ASTM Tribologia e Microdureza

19 FABRIC LAMINATE

Kink-band Failure

Page 48: Normas ASTM Tribologia e Microdureza

• C.V. Opelt; C.S.R. Souza; J.M.F. Marlet; G.M. Cândido; M.C. Rezende "Compression Failure Modes of Carbon Fiber Fabric Scraps/Epoxy Laminates" 20th International Conference on Composite Materials.

• Prepreg scraps plain weave fabric (HexPly® F155) were positioned side-by-side with a random orientatiom.

20 FABRIC SCRAPS LAMINATE

Page 49: Normas ASTM Tribologia e Microdureza

21 FABRIC SCRAPS LAMINATE

Page 50: Normas ASTM Tribologia e Microdureza

21 FABRIC SCRAPS LAMINATE

Delamination

Wedge

Wedge

Delamination

Page 51: Normas ASTM Tribologia e Microdureza

21 FABRIC SCRAPS LAMINATE

Flexural damages

Flexural damages

Page 52: Normas ASTM Tribologia e Microdureza

22 FABRIC SCRAPS LAMINATE

Page 53: Normas ASTM Tribologia e Microdureza

22 FABRIC SCRAPS LAMINATE

Multiple delaminations

Multiple delaminations

Page 54: Normas ASTM Tribologia e Microdureza

22 FABRIC SCRAPS LAMINATE

Buckling of the layers

Buckling of the layers

Page 55: Normas ASTM Tribologia e Microdureza

23 FABRIC SCRAPS LAMINATE

Page 56: Normas ASTM Tribologia e Microdureza

23 FABRIC SCRAPS LAMINATE

Irregular propagation

Irregular propagation

Page 57: Normas ASTM Tribologia e Microdureza

23 FABRIC SCRAPS LAMINATE

Multiple delaminations

Multiple delaminations

Page 58: Normas ASTM Tribologia e Microdureza

23 FABRIC SCRAPS LAMINATE

Buckling of the layers

Buckling of the layers

Page 59: Normas ASTM Tribologia e Microdureza

23 FABRIC SCRAPS LAMINATE

Delamination

Wedge

Wedge

Delamination

Page 60: Normas ASTM Tribologia e Microdureza

23 FABRIC SCRAPS LAMINATE

Flexural damages

Flexural damages

Page 61: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 62: Normas ASTM Tribologia e Microdureza

• The analysis of the compression failure modes is not straightforward and requires some time and effort to be made.

• This kind of information can aid the designers to control the compressive behavior of composite structures.

• The literature presents evidence that for each failure mode a compressive strength distribution can be found.

24 APLICATION TO DESIGN

Page 63: Normas ASTM Tribologia e Microdureza

• The paper of Odom and Adams (1990) shows some interesting findings:

• The through the thickness shear failures are related with the minimum possible compressive strength.

• The maximum possible compressive strength can be expected to be associated with the in plane shear failure.

25 APLICATION TO DESIGN

Page 64: Normas ASTM Tribologia e Microdureza

• Among this two boundaries lay the other possible failure modes.

Narayanan and Schadler (1999)

Lankford (1995)

26 APLICATION TO DESIGN

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Compressive strength

27 APLICATION TO DESIGN

Page 66: Normas ASTM Tribologia e Microdureza

Unidirectional composites (ISS)

Compressive strength

27 APLICATION TO DESIGN

Page 67: Normas ASTM Tribologia e Microdureza

Unidirectional composites (ISS)

Compressive strength

27 APLICATION TO DESIGN

Page 68: Normas ASTM Tribologia e Microdureza

Unidirectional composites (ISS)

Compressive strength

27 APLICATION TO DESIGN

Page 69: Normas ASTM Tribologia e Microdureza

Unidirectional composites (ISS)

Compressive strength

27 APLICATION TO DESIGN

Page 70: Normas ASTM Tribologia e Microdureza

Fabric composites (ILSS)

Unidirectional composites (ISS)

Compressive strength

27 APLICATION TO DESIGN

Page 71: Normas ASTM Tribologia e Microdureza

Fabric composites (ILSS)

Unidirectional composites (ISS)

Compressive strength

27 APLICATION TO DESIGN

Page 72: Normas ASTM Tribologia e Microdureza

• To improve the performance of composites in compression, the failure modes associated with low compressive strengths should be avoided.

• Tougher and stiffer matrices, would lead to the splitting/fiber crushing failures (depending on the fiber arrangement) or even to in plane shear failures

28 APLICATION TO DESIGN

Page 73: Normas ASTM Tribologia e Microdureza

• Introduction

• Goals

• Failure modes

• Case studies

• Application to design of composites

• Conclusions

SUMMARY

Page 74: Normas ASTM Tribologia e Microdureza

• It was possible to group the compression failure modes accordingly to the properties that govern the fracture phenomenon.

• Two case studies were presented to demonstrate how to apply the proposed classification.

• The compressive strength behavior was found for each failure mode.

29 CONCLUSIONS

Page 75: Normas ASTM Tribologia e Microdureza

Thanks for the attention!