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1
ICP Test Report Certification Packet
Company name : Littelfuse, Inc.
Product Series: Silicon Protection Array
Product #: SP3012-04UTG
Issue Date: October 3, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive_2002/95/EC &
RoHS 2_Eu Directive_2011/65/EU) -restricted substance nor such use, for materials to be used
for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing
processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
Global EHS Engineer
(31) Parts, sub-materials and unit parts
This document covers the Silicon Protection Array RoHS-Compliant series products
manufactured by Littelfuse, Inc.
＜ Raw Materials Used
Please see Table 1
(31) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks：.
2
Table 1: List of Raw Materials covered by this report
Total Parts
Raw Material Part Number Raw Material Description Page(s)
1 N/A Leadframe 3-16
2 8006NS Adhesive – RoHS & Halogen 17-21
3 N/A Au Bonding Wire 22-34
4 CEL-9220 Epoxy Molding Compound 35-42
5 N/A IC Wafer 43-46
6 N/A Finished product – RoHS 2 47-51
Form 585-047 Rev. A 2/21/06
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N.D.
arm ol FBB0 mg,eg wlth rcferonc€ to IEC @212008. andmrrotrndd bv GC-MS N.O.
ilonobromouph.nYl mgr(g wlth r€leronc6 to lEc 62321 :2008, dndoertonn€d bv GC-i/6
N,D.
Dibo.mHph.rly n'drs wllh rolsrenca io IEC 62321 :2008, endDedom€d bv GC"MS
N.D.
Tdbromobiph€nyl nte/k0 Wi$ ret€renco b IEC 623212008, anddtr6m.d bv Gc-Ms N.D. 5
l€trebromoblph€rlyl mg/(c-friifr-&r€nc€
to lEc 6821 2008, ardmn6tm.d bv GC'MS
N.D. 5
lbxabromobiph€ni msac wlr'h f€Lrgnc€ to lEc 6232'12fi)a, andD€rfomed bv GC-MS
N.O.
Ponteb.ornobiph€nyl mgrkg wnh retursnca to lEc 8iB2'l200a, andD€fom.,cl bv GC-MS
N.O.
H€gtabromoftPhonYl mgr(9-Wifrflr€nc.
to lEc 623212004. ando€nonnod w Gc-MS
N.0.
dabromoblphony| mgr(g with lrl,ar€nca to IEC 623212000' andmdolm€d w CIC-MS
N,D.
NonabromoblphenYl msao witr oterenco o EC eagzt eOOg' anAo€rtonn€d W CiC-MS
N.D.
O6c€bromobiph€nyl mdxg Wilh retarenc€ to EC et3211008' ando€fom€d W GC'MS
N.D.
r.5(S)5121 232i, 1.6{03}5121 l$2 |*rrsd
& n ot PBOEa mclQ with rdterenc€ !o lEc 6fi)21:2008. andert^n .l lw l!a:-MS N.O.
Monobromodiph€nyl €lh6r mc/xo wi$ reiarenc€ to l€c 6fr,21:2008. andoeforrrC W GC-MS N.D.
Dbromo<,iplBnt aftgr mgao with rslsr€nco !o IEC 623212m8, ando€riorm€d bv @-MS N.D.
TribomodphenY e$€t mgkg with relorsnce to IEC 62321:2(x)8, andrE Llme.l lw alll-Ms N.O.
Tatabomodiphenyl €ther mcn(s With refer€nc€ to IEC 62921:2008, andmrntnrdt Iw GC-MS N.D.
Pent bomodipheny ether fto/l(| with rghronce to lEc 62321 :eto8, anddrhrrndl tr @-MS
N.O.
tl€xobrornodiphsnt elher lrr919 wih rel€@nce to lEc 62321 :20018, andofftomed bv @{r.ls N.0.
H€FLbrornodDhon, strsr mc/*o Wih reference b EC €Atel:2008. anddrft|rirE l rw GC-MS N.D. 5
Octebrornodiphont ehor m0a0 with €lolence to lEc 623212008. ardo€rfo.m€d W GC.lrS N.D, 5
tlonebromodiphony' 6fier rncko wih r€felence to IEC 62921 :2008, andD.ioflrbd w GC-MS N.0.
oecabomodhhany atrtr meAo wi$ referonco to IEC 62}212008, ando€rlom€d W GC-MS N.D.
Test Report tb. LPqnst84B)n 1.r\A2ltll/81388 D.t : 0z12r2l'1r P.g€: 3 ol 13CIS Ret. CT911/,*t39/t nd(.
Note : (a) mo/kg - ppm ; (o.twt% - l000ppm)(b) N.D. - Not oot€cted(c) MDL - Molhod Detecllon Limit(d) r - sDor.T.3r:
a. N€galive means lh€ eb3enc€ of C(vl) on the lesl€d eroasb. Posltlve means the presenc€ of C(Vl) on the t€sl6d aroag(Tho tslted sampte should be tunhef verifrod by bolllng-wateFextraction melhod it lhe spott63t rosult ia n€galive or cennol b6 conllrmed)Solllng rdaa axlracllon:a. Negativa means th€ absenc€ ol C(vD on lhol9gl€d areagb. Posltlve means lhe presence of C(Vl) on lhe tesled argaS;
The ctelocled conc€nlfatlon ln 50 mL boiling water axtrectlon solution i3 equgl or gfeaterUun o,o2 ng/kg wllh 50 cm' sample surfaco ar€a.
For coroslon protoclion coe$nos on mota|3: Informalion on storag€ clndltiorc and p.oducllondatq ol the t*t€d sample is unavoilablg end thus resultl ot 6(vl) r€presed statu3 of th€sampl€ al lhs dma of tosting.
(€)--Nolregulated
SGS LABORATORY SERVICES (M) SDN. BHD.
CHONG KIEN LENB.Sc.(HONS)AMICLAB MANAGER
fu|_.biedi.!frr'e
;;-fr ;;7-a ;l;"1 i -_fi Effi -i_ j5btu;6!i;'i-;;-ri.idl;rbiFind
scs L.bd.br ss{6 (L) sd' tsn{C{!l,rb6372l4
ib26 Jtr Ar{gdl vailb 31/!3 l(ob l(mnhg {4{60 sdrla D.ir E|M.1.6(0q5ia ?'2o l'5{03) 5121S2 fl5sFm
scsTest Report No. LPCt25l3qBy1l+K,lA)ll/91388 Dato : t}?I2rZ)ll Pago:4 ot 13
CTS nd. CTSfl 1/45i19/T.[t!
Te€'t rEsllts by chornical rh6thod:
T..i [.m (!): Unn llethod Rra{lt !9!
Andrmny (Sb) ppm wilh rel€rencelo EPA Melhod 30512.and p€rfodnsd by lcP€Es N.O.
Polyvinylcfi bril€ {PvC) Analysis v|as p6rtom6d by FT-IR/ATR Negaliw
lhlogcn
Halog6n-Fluorln€ (F) rto/xg W 11 €f6r€nc€ !o 83 EN 1,L582. AnelFis wagp€domed by lC melhod ior Fluoine conl€nl. N.O. 50
Habg€n-Chbdne (Cl) mg/ko Wlth r€l6r6n e to BS EN 1ut5l2. Analy3b we3podom€d by lC mgthod lor Cnbrjno conienl. N.D. 50
Halog€.-Brodine (&) rlryks wth rg!.r€nc5 to Bs EN 1,1582. AnelFis wespo ornod by lC rn€0|od for Blomln€ contont. N.D. 50
Halog€nlodine (l) m0rk0 with rolslence to BS EN 14582. AnalyaiB wasp€rfom6d by lC nafiod tor lodine content. N.0. 50
I9g!a4.9esc!D!ie! :
Samplg Doscrlption Au Bording Wire
Note : (a) mg/kg = ppm(b) N.D. = Not Dot€cl€d(c) MDL - Mothod D9t€ction Limit(d) ..- = Noi conducted(€) " = Ooatilaliv€ amlysis {m unit)(i) Nogdtuo = Und€t€oiabl€ / Pogitive - Dotoctable
SGS LABORATORY SERVICES (M) SON. SHD.
CHONG KIEN LENg.Sc.(HONS) AMlcLAB MANAGER
Br'4-_:.@r
iF.;.*-*i;;Ana.
1526 J.!.i lrlgqik vdilb 3103 (.a! iemr! aol60 s.lrtd D.nr Bs, rabvlrl1.6(03)512!2310 r{(a)5121S2 |w.tssor
SGStzacio.yss{a{ )Sdt e'd(CdiF r$ 6s72rl)
Test ReportT93l result:
Lesl.PlB-Qtrlllhlig! :Sample Doscridion
ilo.lpc 25l32(B)/t l +KA/:ml i/81388gf S R.t. CtE4 I l$30/f andc
ttatc : 02'l2f20ll Pago:5 ol13
: Au Bondlno WireOidoml: Foll8 Olrrc0v.2011i65/EU. odorltv !ub!t nc..
Note : (a) rng/kg = ppm(b) N.D. - Not D6t6cted(c) MDL = Mgthod Delec{ion Limit(d) --- = Not conducted
SGS LABOMTORY SERVICES {M) SON. BHO.
sGS L*o.rblt Sqtc (r0 s(h Bli.(ctFyrb 637lrl
CHONG KIEN LENB.sc.(HONS)AMICLAB MANAGER
*ffi6d.nhbc-rr . ; l6r. t rr !6bl-s! 'Efd'ddcr|dh
!026 J.hn A,&t iLvdaa 31t03 r.ott (gDnb! 40460 s€Lild o.ni Ehen M*vs, ! .€{@) s121 2320 i +6 03) 5la w m3$@
Test h6m(s): Unit Tg€t Motlod R6sufls MDL
HerEbaonroc).dodod€can€(HSCDD) msas Ba!€d on IEC 62:i212008. and o€rbm€d
by cC-M{; N.D. t o
Ptdhahl .
OBP (Onbdyl phlhalat )(CAS tlo.: 00008+7+2)
Wilh r€ter€nc€ lo Chromalographla Vol,47,No.78rt, 1998. Analysls was p.ilorm€d byGC/MS.
N.D. 0.003
DEHP(Oi"(?-€lhthoryl phttalate){CAS No.:000117{1-7)
Wlth lgtercncs io ChronaiogEphh Vol.47,No.784, 1998. Analysk wes porfofii€d byGttl/Ls
N.D. 0.003
BAP (86m, 8uV phthelaro)(CAS llo.: 00006S0-A
wlih rofdBnce !o Chfomaloorephla Vol.47,No.784, 1!X)8. AnalFb sas p€rtom.d byGEUS.
N.D. 0.003
DINP (Oi-honon, phthalato){CAA No.:02855&12{) %
Whh roleiEnca io Chromatooophla Vol.47.1,10.784, 1998. Analy6b wes podom€d byGClrrs
N.D, 0.0r
DIDP (Oi"i.od€cyl phhalalo)(CAS tlo.: 046761-a&0)
wllft r6f€r6nc6 to Chromelographla Vol,47,No.784, 1998. Analysb ras pedomed byGC/MS
N.D. 0.01
DNOP (Dl-n{dyl phthdate){CAS No.: 00o l I 7{4{} %
\lvlth referenco to Chrorhaioo6thla Vol.47,No.784, 199& AnalFis yras p€rfomod byGaJlrS
N.D. 0.003
DNHP (Di-n-h.xyl trth3lete)(C S No.: 0000€+753)
Wilh rolgrencg tic Chromatogr.phia Vol.47,No.7&, 1998. Analy6ls naa poriorm€d byG(rl/ts
N.0. 0.003
Test nem(s): Unit Test Mehod Results ldlt
'Pfio€phorus (P) ms^€Wilh rebrenco to US EPA M€frod 3052 for
Phogphonl6 Contenl. AnalyBis waso€rionnsd bv ICP-AES.
N.D.
S€Mlium [Se) rnoagwih relerence t0 l,rs EPA ir€hod 3052 hrSoryllium Cont6d. Analyaia wa! pgdomad
bv ICP-AES6.64 2
'[&ono!tium ([,lg) ntg/kowlh rofargnc€ to us EPA llloftod 3ts2lor
It&on€3ium Cont6r{. AnalysE $aspodom€d by ICP-AES.
N.D.
'Paalluorooctane sulionatea(PFOS - Acld, ti,lotal salt, &ni&) msAs
wift roiaronc€ lo us EPA &ttoc: 1 996molhod for PFOS Co ant. Analysb wa3
o€dornrd bv LOUS.N.D. 1 0
' PFOA (CAS tlo.: g15-67-1) mgrlswith retsfsnco to us EPA 35toc: 1 996mghod lor PFOA Conibnt. Analysis was
brllm.d hv LdMSN.O. 't0
'Dlrn6thY Fumareto (CAS t'to.:62449-A ncks With €lerence !o US €PA 3540C m6$od.
Analysb wa8 perronn€d by GCA4S. N.D. 0.1
'DMEP (tlE (2-m6tbxy6thyl)phfisht€) (cAs No.: I 1 7-82-g)
wllh r€t€rgnc€ to EN l,ls72.Anelygis wesp€dom€d by GqUS N.O. 0.m3
Test Report
Nol€ :
No.IPC :l5l34Byll+t(A/:XI1iBt360 Orte:0zt2rzt11 Pagcr 6 ot tgCTS Rlt Clgl I /45i19/Tand6
(a) mg^g . ppm ; (0.1M%. 1000ppm)6) N.D. - Nol D.tect€d{c) MDL - lr€lhod D€t€ction Limit(d) 'Tho abovs teets ssre lubcontractod to SGS Taiwqn baged on roport no. Kl,/2011/81388
PFOS R.iEr.|E InlomEdon : Dlrrcllyr Z)06n22/EC(1 ) May not bs plac€d on trte mad@l or u6ed a6 a subslance or coGlrtusnl ot propaEtions in a
concentraton equal to or higher than 0.005 % by n€ss.
(2) ti,tay not bg plac€d on lha market in s€mi-finished poduc,ts or anicbs, or pa|F theraol, ff thoconc€nt aton ol PFOB b €qualio or hlgh€r then 0.1 % by mess calculat€d rrith referenc€ to themass ot siuctulally or micostucturally distinct pqlts that contarn pFOS or, lor t€xilles or othorcoal€d mat6dals. if th6 amount ol PFos is equal to or higher lhan l pg/m' ol lhe coetEd inatedal-
SGS LABOMTORY SERVICES {M) SDN. BHD.
CHONG KIEN LENg.Sc-(HONSIAMIcLAB MANAGER
6G3tsoobys6roer{M)sd' lhd ' is26JasrA|EEeilvhilb3l/Slot xmaElOLOS.lildDaol€16a., ulLFd(c{r!.ryr$ 6}9?2.14 l.a{03)5121 2320 r.6(03)5121 9032 ffir$tm
scsTest Report Dalo : 02y12/2011 Pag6: 7 ol 13No. LPCff25132(B)/l l.l(A,/a)l1/81384
CTS R€4. CIS/'! l /4539/Tanakr
I.eglerl-pesgrlAis :
Sample Oescaiption Au Bondlng Wire
SGS LABOMTORY SERVICES (M) SDN. BHD.
8GS L*.dtory S.ncs (M) sdr Bhd(CdFylL GB72.I4
CHONG KIEN LENB.Sc.(HONS)AMICLA8 MANAGER
@'4qq!4o4t)
tu;;;4d;b,flqriiir'dd-;nr6c*rr l l r l4 l ,
l{016 JaL. At!{€il Vdilb 31/st Kolt KmnhO !|0160 Seb{o 06rulEren, M.bts6I .(ts) 5121 2320 | '6 (03i 5121 9032
"*{F.m
SGS auihsntical€ lh€ pholo on the odginal r€port only
Test Repofi
1. 9E!4!!4!q949!!!JEeq!E!I.9!llc-@unos
Sampb R€c6l$T arld R.gb!e!o.t
qd sando h 6m.ll pl€c€!\,
W.lghl Benpl€ {0.2.0.5{} Inio dop3lon v€.3€l*
Add dlEotbn (Mcro*avo)I'Iorally Dl88olv€d'u
Fnrdion+
Arutg€8 br rcP
3. E!E4!q!!Q!.@EEC!JE:|@!!E!I9!Ec.!ell300!
ssmplo F€c6h/n9 and R.gbtr|ton9
qn samds In smal dscsr,
w€iehr 3dnpl6 (02{,lg} iiro dgscdon \,6i.61J
Add dg6to. (rub'otEw)\,
'Iotaly Dbsoh/scJ
F rdonJ
Amlya€8 bt ICP
5. DEIEBIIIAIIQI9EIIEIPEDEUI!.9&T9!IJEC.@ri@
Cul aendo In 8ruI d6co3
w.ig lamdo (0.ta.09) l.io €xr.ctbn lhlmu€
sot{ol E tacld' silh T0lr0.'€I
Fllt€r tlxloCh 0.45 um mombran€ fn€r
Anatyse by GC-lrS (nrdth ryrogide dMon)
SGS LASORATORY SERVIC€S (M) SDN. BHD.
{o, LPClrl5l3qBy'll+{ All1/B1388 atato : 0Z12rDt1 P.ge: 6 ot 13CIS Brl. CTgl l/1530/Tand(.
A DEIEEU|IAIIqT.OiIEAD.SOTIENI-EI!89-!@!-?@
Samdo R66dlvtry and Roliln'dion
qx samd6 ln cmall rt6c6
WdCh eamC€ 024.5{) inro diqErlon v€ssol
Add dlg€droo (Mcroi,avs)+
'Ioralh Dbsolv€d'+
FI[ratbn
Analyl€o b'v ICP
samd€ R€Grvirtad B6d.rran'n
srnd0 P.€parallon
seoH€d fuaxrdrv€)
Adhg-uialor€ttacilon
An.lF€. hy W. yo.r lopholomglor
f6rt F€pon
7.@!Ir|Etl!!E
Sample PrcDaretont
Hol wal€r orLacton+
,dd ooituri.v€lodng €ag8nlt
L6i sland lor tlo minJ
Analys€o by W- Sp6ctopholont€lsr {5'lo nm)
CHONG KIEN LENB.Sc.(HONS)AMICLAB MANAGER
dt.ddbbbrooqE5i:€:!;ffi
j!bdr-"r*n .qd@cd&r-;Acid-irb*;;-5;*ddnG.,4-E@Edtrb-oir4;994*-r.-.i r!!:!*:11::!'!:'tedebdiil#;R-td.*_#:;;'w-=.-d;iffi ;;&-;;;;_--5'!!!-h4'n;Fda.*i
6C'.t&r*.yS€rvE(M)8(!| Bri ib26J6Arlldkvalb3llt3K.at(gMrgloltos.hgdD.rulElo^(cdqrr$ 6rm.$ !llPl5lr-t_4? r.6,03)5121 0062 Iwslsd
Test Report
at!!Eg!4gE!sE!t039!q!!qE9!t9!.0!W
OEIEA.SCIICut aampla In small plsc€a
tW€irm sampl€ (0.2{.!g) ir o d(toslion veesol
Acid diOoEton (HF snd 8Nq) - Mloro/yav€J
"Totally Dbsolv€d'+
Fin ation
Analy363 by ICP
No. LPClZtsl3qByl I +KArAtt 1/81388CTS Fot, CTgi 1/45i19/Tanrk!
Oalo i02/12t2o11 P.gp:9 ot 13
e. 9E!E!!!4!!g!.94!q94ggqEU!
Stmplo prelf€ah€nl
Wolghdng and puning sampl€ in call
Conbuslion / Absorpdon
Dilution to fx€d volumo+AnalF€s by lC
1 0 . @
Cul sample in small piecosJ
Sahpl€ snelF€d by FTIB.,
Dala
scs LABORATORY SERVICES (M)SDN. BHD.
SCS L&iloiy S.nd3 00 8d. Brr,(CdFryrs 6t?2r4
lo2oJ.b.A,tqd*valb31/to|G6Kdnd{i(''160&b4dD6nlEh6ti Mabtst.5{03) 5121 23a} r'6(Ol)51219032 ffi!{s.tr
CHONG KIEN LENB.Sc.(HONS) AMICLAB MANAGER
lffiffi-t*P.d"*-3!!e.@ q-E;|;d;ff;d/-i;tu-d4 ft @-cE.;;d:-F ;:q';bd-.- '*! '
;];J6;*6tudddhh*d#*c'|
Test Report l|o. LPqn5tu(8y11+l0rAnl/81388 Dtt : 02y12!xr11 P.g€: l0 ot t3CfS nel. CTgl i/4$O/fanat
1 ) Ths€o eamples vrere dissoved totally by p.e-condilioning melhod accoding lo below
2) Nam€ of the p€rson who madq measuram€nl: Alex Chang3) Name of the peGon in chaqp ot measuremefi: Ray Chang
Flow Charl for tho elamenl! analysls porform6d by ICP-AES
Sl€€1, copp€r, alumlnium, soldst Aoua resia. HNq, HCl, HF, HrO,
Glase HNO3/HF
Gold, plalinum, palhdium, ceramic Aaua r€g|aSilwr HNO3
Plasuc H,SOa. H,O,, HNq, HCI
Others Anv acid to totat dioestion
scs LABOMTORY SERVICES (M) SDN. BHD.
CHONG KIEN LENS.Sc.(HONS) AMICLAB MANAGER
fb28ldbn Ar4arr vruL !1rs Kot xmnig a0{60 6eLi9d lbrulEIMt.8{l}3) 5121 z}Xl 1.6103)5l2lw MqF@SGE Labodioq Sdna (Y) Sd. Bhd
{CorF 15. 53s7r{4
Acid diggstion by suitabls acld dep€rd6d ondilfsGnt samde matorisl (as bslow table)
I ) Atkali Fusion2) HClto dbsolv€
Test Report No. Lpd/2513q8y 11+Ktixtt l/B1388CIS R6f, CTgl I /it5oo/fanaka
Analytlcal flow chart ol PFOA/PFOS conlent
lrrte :(}2/122011 Pago: 11 ot 13
t ) l.lam€ ol th€ p€asoo who made meaelrsm€nl: Anson Tsao2) Namo of ths ps6on in chargo of moasurement Ray Chan!
SGS LABORATORY SERVICES (M) SDN. BHD.
CHONG KIEN LENB.Sc.(HONS)AMlcLAB MANAGER
5rdffi,*E 6s.E4r4.E4ql
fi;;ciff idr-idd d - - r t b c d l ! . E q , t t t l d l b @ . r d d e t d h
6GS L.aord.ry salc M Sd BM rh26$bna,gar va|b 31lg3 K.b KmnrE 40{& Seldgo. Dodr Eb.i MabYe
{cdF,yr$ &lzra t.6(6)5121 2fl1 1.6(031 5121 90@ m3F@
Samde pr€tr€almgnt
Sample oxtraction by soxhlgt extraclion(Retorence mottrod US EPA 35/rc)
Analysls was porformed by LdMS
Test Report
CHONG KIEN LENB.sc.(HONS)AMICLAB MANAGER
AnaMlcal fow chart ot Dlmothyl Fuma.ate conlent
Drte: O2/122O1'| Pag€: 12 of 13ilo. LPCt25l32(E/1 1+KA/201lrBl3aECIS Rot, Clgl l/4qtgTanakt
1) Narne ot he De6on who nud€ niea6uEment: Anson Tsao2) Nafi|€ ol tie p€6on in charge ol FEsurernent Ray Chang
SGS LABORATORY SERVICES (M) SDN. BHO.
iii.;b;*&i;i;;a.iwtadtlrdr*!b*
6GS L&rdortS.Na.s (M) 6ih. Bhd. , rbr6JtltnArOq€nkVmilb3lA3KotaXm.i4.l0a60S.b.!Froordtrdn, MtLv$(cdFyNc6€?2.14 t'6(@)5121 232! 1.6(03)s121 9$2 |*iesd
Sandg orelrsalmont
Samplo extractlon by organic solvent
Analyds rvas p€rtorm€d by GC/MS
Test Report ilo. LPO25l32(Byt l.KA/20ll/81388 Dat : Czn Ziml1CTS R€1. CTgl 1/4580/f.nrk
Anslytloal llow chan ol phthalde co ent
1) l,|ame ol tha oo6on {yho maclg mEasu€n|€nt: Anson Tsao2) Narie ot th€ p€rson In oharge ot measurefiFnt: Ray Chang
Data
Pag€: 13 of 13
SGS LABORATORY SERVICES IM) SDN. BHD.
CHONG KIEN LENS.Sc.(HONS) AMICLAB MANAGER
L5-fu5fri*tdi. ' ff i
ddrihr-c-{t. i |t&['qfuGal't*@6.bLfu
scs L.h@ioiy SdMB {U s(h 8hd No26 J.bn Ar{s.r* vtild 31193 l6lt xeMig 4{}{50 s€bnga Darul El\ei, Mabvso(cdir'!yr$.6oz{). .raq!3-)51?JP 13{9.15111w.:Yl,$.*
Sample prelrealnonvsoparalion
S€rnd€ exfaction by soxhlet method
Test Report No. : CEl2O12l428O4 Oate:2012104125 Page : 1 of I
HITACHI CHEMICAL CO., LTD.1772-1 KAMKUBO YUUKI-SHI IBARAKI, 307-0015, JAPAN
Validit nownFor QuesfiPlease Co ith scs
il|lflt lfiI|Il fl
The following sample(s) was./were submitted and identified by/on behalf oflhe client aa:
Sample DesciptionStyldltem No.Sample Receiving DateTesting Period
EPOXY [/|OLDING COMPOUNOCEL-922OHF2012t04t16201 2 I O4t 1 6 r O 20 1 2t 04 n5
Test Result(s) : Please refer to next page(s)-
own'nihhiesieeod6ibroirvrorheemoe6rFned rh srsdrcponenn
i r i sa i , on iens , * ' . " r ydc "Dd ; ' ' ' o ' cdbBLmdd 'o6 l f sds " f u ' " pnn [email protected] |avo |obhsfq b eredonrc bManamds *o&rGTemsand .oldior.to | fti.;d;liiJiiN'i"d;;;di.n;nij;icnonidesdeimdir€cnfu'hddero|hsdeUmed'iadv9d6ah " ; ; " i 6 ; I ; n ; " i ' " * i ; ' , d ; i f $ ; ] i i i 6 ' c i 6d !hsec | i os ' i i ] ^ ! l h comFa '$e ram€b ! ';a;;A dn rcm a;L'm . mndo do e i -i .oLm"i' r'{;od rpad eddcdp l i!o pa-y +y ..u ro' /;o Jr.ano oq-y o' " fr6to o 1" ,rt1r o
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SGSTest Report No. : CEJ2O12142804 Dale :2012104125 P a g e : 2 o f 8
HITACHI CHEMICAL CO,, LTD.,!772-1 KANAKUBO YUUKI-SHI
Test ReSUII{S}
PART I{AME No.l
Test ltem(s) Unit M€thod MDL ResultNo.l
Cadmium (Cd) mgikg Vvith reference to IEC 62321: 2008 andperformed by ICP-AES.
2 n.d.
Lead (Pb) mgKg With reference to IEC 62321r 2008 andperformed by ICP-AES.
2 n.d.
Mercury (Hg) mg/Kg With reference to lEc 62321r 2008 andperformed by |CP4ES.
2 n.d.
Hexavalent Chromium Cr(Vl) mg/Kg With reference to IEC 62321: 2008 andperfonned by UV-VIS.
2 n.d.
Antimony (Sb) mg/Kg With reference to US EPA Method3052 for Antimony Content. Analysiswas performed by ICP-AES.
2 n.d.
HaloqenHalogen-Fluorine (F) (CAS No.:14762444\
mg/Kg
With reference to BS EN 1458212007.Analysis was performed bY lC.
50 n . d .
Halogen-Chlorine (Cl) (CAs No.:22537-15-1]
mg/Kg 50 n . d .
Halogen-Bromine (Br) (cAS No.:10097-32-21
mg/kg 50 n . d .
Halogen-lodine (l) (CAS No.:1436244-A)
mgKg 50 n.d.
Sum of PBBS
mdkg With reference to IEC 62321: 2008 andpertormed by GC/IMS.
n.d.
Monobfomobiphenyl 5 n.d.
Dibromobiphenyl 5 n.d.
Tribromobiphenyl 5 n.d.
Tetrabromobiphenyl 5 n.d.
Pentabromobiphenyl 5 n.d.
Hexabromobiphenyl 5 n.d.
Heptabromobiphenyl 5 n.d.
OctabromobiPhenYl 5 n,o.5 n.d.Nonabromobiphenyl
Decabromobiphenyln.d.
fld:""lii*iti;I",rtj';iii'*1*ft-i"""n#iillisttllii*ri:lX*;"i*:i"i:l;#;fft*"iip; '"'i*,r,*;*r anaoftnoesmat be PrcFared ro
]ttI |||ll I|llllllIBARAKI. 307-OO1 5. JAPAN
DARK GRAY LUI'P
, , sbr l r ranD i .&0r r@ r t d^s '
conpan'Anyunauiro0zeda]le.a!on.bfgelyol
Test Report No.:CE/2012l42804 Dale:2012104125 Page: 3 of 8
HiTACHI CHEMICAL CO., LTD.1772.1 KANAKUBO YUUKI-SHI IBARAKI, 307-0015, JAPAN
NoG :1. mg/kg = ppm I 0.1wgo = '1000PPm
2. n.d. = Not Detected3. MDL = Method Deteclion Limit4 . " - "=No tRegu la ted
flr|iIlrl0 mt !t1
ffAi:,ffi#;1ffi:$,ffi;i-=ii'iE#;':l:i;5ii':i:'rr"":e1ir'!i11'"s':@fr--de@'d*'d"*''i''*-'^'**^-*'*"'*hffi-}h:#t;{"}.T,*$?3,|nfi$iE$tr..:$H:$j*!#i,1!F;'sjtr#.j$*{flt$3.ififf#*u$T,;ffi[hffi,t1ffi$jffi
Te3t ltem(s) Unit Ilethod MDL ResultNo.1
Sum of PBDES
mg/kg With reference to IEC 62321: 2008 andperfomed by GC/[,]S.
n.d.
lVonobromodiphenyl ether 5 n-d-
Dibromodiphenyl ether 5 n . d .
Tribromodiphenyl ether 5 n.d.
Tetrabromodiphenyl ether 5 n.o.Pentabromodiphenyl ether 5 n.d.Hexabromodiphenyl ether 5 n.d.
Heptabromodiphenyl ether n.o.Octabromodiphenyl ether n.d.
Nonabromodiphenyl ether 5 n.d.
Decabromodiphenyl ether 5 n.d.
Test Report No. : CEl2012l42aa4 Oale :2012104125
HITACHI CHEMICAL CO., LTD.'1772-1 KANAKUBO YUUKI-SHI IBARAKI, 307-0015. JAPAN
1 )
P a g e : 4 o f 8
Sample Material DigestionAcid
S-teel, copper, aluminum, solder Aqua regia, HNo3, HCl, HF, Hro,
Glass HNOy'HF
Gold, platinum, palladium, oeramic Aqua regra
Silver HNOs
Plastic H,SO{, H,Or, HNO3, HCI
others Any acid to total digestion
l n I ||lmll$llll
2',13)
These sampleswere dissolved totally by pre_conditioning method acc.rding to belowflow chart( Cr6* test method excluded )
Name oflhe pe6on who made measurement: ClimbgreatYangName of the person in chafge of measurement: Troy Chang
ICP-AES
Cutting / Preparation
Sample Measurement
Add appropriate amount of
digestion reagem
Microv/ave dige6tion with
HNq/HCVHF
Acid digestion by suitable aciddepended on different samPlematerial (as below table)
Heat to appropriate
temperature to eratract
Cool, filier digestate
th.oughfilterAlkali FusionHClto dissolve
Add diphenyl-c€rbazide for
color development
measure the €bsorbance
at 540 nm by UV-VIS
Cr5.
r a s r o - t r e t 7 4 - i ! 9 5 4
scqTest Report No. :CEl2O12l428O4 Date:2012104125 Page: 5of I
HITACHI CHEMICAL CO., LTD.1772-1 KAMKUBO YUUKI-sHI IBARAKI, 307.0015, JAPAN
1) These sampleswere dissolved totally by pre-conditioning method accotding to below ffow
2) Name oflhe person who made measurement climbgrcatYang3) Name of the person in charge of measuremen! Troy Chang
Flow Chan ofdigestion for th€ elements analysis p€rformed by ICP-AES
Seel, coppef, aluminum, solder Aqua regia, HNO3, Hcl, HF, HrO2
Glass HNOs/HF
Gotd, platinum, palladium, ceramic
Silver HNO3
Plastic HrSO{, H,O,, HNO3, HCI
Others Any aoo to lolaldigestron
yp-t:ll-";, .,.. - ^ "";1,";" .,",.:." *
""*.! -1,;lt:"t;;:;::*:".""f, ffi *,;;'^l* ,"?!1.:;,c""Ti.:t: :,jA o*"i".1,i,*';",i...,"::i:F ""1"a n d | o r e d r c m i o m a l d o c u m e d s s l b F d ] o T m s a n d c o n d i 6 s. : ; ; . d | h l | ' h " " " . ' f ' * . J d u E d q * G ' o a T o I ' ; ; ' ; : ; d o , | ' d ' f i d j d ' * d
.;:'m:li:,1{.."'*;rrfi$:d,,i;ll"r#.*;,";"r.i fii;;"#i-"*i:*';!Jra#1i;:r;"tir:ir':t'ffi":rri;'r'g;;
r!fltu [lllLi:
Test Report No.:CE1201?J42804 Dale 2112tc/.125 Paoe:6of 8
HITACHI CHEMICAL CO., LTD.1772-1 KANAKUBO YUUKI-SHI IBAMKI, 307-0015, JAPAN
llllt [tll| r[ul tt
Analyticalflow chart
r Name oflhe peEon who made measurement Roman WorLgI Name oflhe person in charge of measurement Troy Chang
( Test ltems: PBB/PBDE, TABP-A.bls )Firsltesling prccess -----.> Oplionals@en prccess ..!t Conlimation process - .>
Scrc€n analysis
Sample extraction method
ConcentratdDiluE Eliracled solution
vI Analvsis bv GC/MS I
v
pany subjed io ib GeneJa condtuib l { r ' o - q , d r c . o d r " o " T . . o n , . - - | s ; o - o o d f l . o T
miratoiorrabiit 'ndemficaron and y horder oftt i s de'nad iaadv sdd rhr:, iy rhe comp3iy! $re respodtb i 'ry s 10 ib c enr.id rh! d@ment does nor eroieEG padi.tro.
qaned on irm e,eEs ns a Ldnscto,i dodmenG li6 dcmenr 6id ha .ep6du€d er@pr i tur wbou pior Mr6n aprioyaLor rhee lu erene o1$e e
Test Report No. : CFJ20'12i42804 Oale | 2UAU|25 Page: 7 of 8
HITACHI CHEMICAL CO., LTD.,1772-1 KANAKUBO YUUKI-SHI IBAMKI, 307-0015, JAPAN
Analytical flow chart of halogen content
1) Name ofthe oeBon $to made measurcment Rita Chen2) Name of the percon in charge of measurement Troy Chang
rfll|[ll|| lu[ ||t
Weighting and putting sarnple in cell
Oxygen Bomb Combustion / Absorption
DilLrtion to ixed volume
Analysis was performed by lC
| l . r " : ' , . j ' ' ' , ' ' ' . "^ ; " ;e" ' ' . . " " ; ' " ' : . . l . i i . " " . , i " . ." : d ; : ; ; ; n ; b ; ; ; o l F 1 ' * b 1 - | 6 - e r u f d . o ' d ] mh h ; d ; . i b l ' i N : f d . m I i l i € b n a i d ' t d d m i s c s d € f i m d I h g ; n r i i ' a ' d b 6 d @ u r e d , i d , * d h
[;;{i;til'n::;'"';*'#i$,iiifiii*i+:';iitif:"s:}l:,-'J'"ir:llqx.lirir:3J}'*i"""-"ji"tjil:i:"jjtj {i:i1'";ri"';j:t"'j
IscsI
Test Report No. I CE|2O1A42804 Dale 2O12lUn5 Page:8of8
HITACHI CHEIVICAL CO,, LTD.1772-1 KANAKUBO YUUKI.SHI IBAMKI, 307-0015' JAPAN
' The test€d sample / pad i6 ma*ed by an arrow if ifs shown on the photo '
" End of Report -
ffihffiffimNffiffft-,,ffiemmiffiffi
rlfl||[||l[[llll
42804
Test Report No. : CEl201z12U2 Date: 2012t01t18
EPISIL TECHNOLOGIES INC,NO. 3, INNOVATION ROAD 1, SCIENCE BASED INDUSTRIAL PARK, HSINCHU.
: As specified by ciient, with reference to RoHS Oircctivedetermine Cadmium, Lead, I\rercury, Cr(Vl) contenls in
: Please refer to next page(s)
Validit nownFor Ques-liPlease Co ith sGs
P a g e : 1 o f 4
2011/65/EU Annex ll tothe submitted 6ample.
ll []|llln||[I||lTAIWAN, R. O, C.
Thefollowing sample(s) was/were submitted and identified by/on b€halfofth€ client as:
IC WAFERALUI\,/lINUIU PROCESS2012101t112012/01 t1 1 TO 2012t01 t 1 I
To6t Requested
Test Result(s)
Sample DescriptionStyle/ltem No.Sample Receiving DateTesting Period
t{b.Cgmd forsGSIAIWA
{Nw4p
Test Report No.: CE|201Z12U2 Date :2012to1t18
EPISIL TECHNOLOGIES INC.NO. 3, INNOVATION ROAD 1, SCIENCE BASED INDUSTRIAL PARK,
Paget 2 ol 4
t [t! [t]||!fHSINCHU, TAIWAN, R. O. C.
Test Result(s)
PART NAME No.1 I,/]ULTICOLOR WAFER
reference to tEC 62321:7008-ind-
ith reference to tECG2giJ26dEEiled by ICP-AES.
reference to IEC 62321:7008cna-
Hexavalent ChromiuFT rence to IEC 62321i 2008 andperfomed by UV-VIS.
Note i1. mgikg = ppm : 0.1M% = loooppm2. n.d. = Not Detected3. iIDL = l4ethod Detection Lamit
i lF*f i" ^ : '*t" ' ' " 1* r" *1 '- ' ; :e e?erTlo"b.t*erq1" * ' :". . . : . t---
.r":.rni{.":: f.4-:|.li:,11';,"1",1*.l]:."":;1.""-%e-.'""*:e;6:":"rf$:ffii",..,j"".+;pf::B^rt ;e;*S;o;.,-".:; i"{"".f;:*T;;;!"-; ilE"" .'t;,;*fi;ly:t;fl:,;';:"s.;:f.";/,,39;3:i,.i,-";x.dr;r:;st :3h.s;;i:_i"; t';_1;;-*"1::: ll i:"iui.,;;.;1.]ii",T*:'"i9li.::t.'s"'".:;iJ"oiidt:x,?i;rf,,";:::";",;"*;:;j.-.,.#;"{,i":*",:h,r*j;i,';l;gjj::r_;{,pll}::
Test Report No. I CE|2012J 12342 Date :2012t01t18
EPISIL TECHNOLOGIES INC,NO. 3, INNOVATION ROAO 1, SCIENCE BASED INDUSTRIAL PARK, HSINCHU, TAIWAN, R.
ICP.AES
Sample Material DigestionAcidS'teel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,Glass HNO3/HF
Gold, platinum, palladium. ceramic Aqua regia
Silver HNO3
Plastic HrSO., HrOr, HNO3, HCI
Others Any acid to totat digestion
Page: 3 of 4
rr[[ t|| ]l|tI|o. c.
1) These samples were dissolved totally by pre-conditioning method according to below flow chart.( Cr"' test method excluded )Name of the per6on who made measuement: Climbgreat yangName of the person in charge of measurement: Troy Chang
2)s)
{rlii:fli'J: i:f '".i'iif iigl ii.T:ii:r 5H .:r:[:"]ri,:ii*ri'ji!' j.:e1i!i:,F.jr*" -*" * *.".
, . 4 "db a c€Tu , cdo i r o re d ,Nc o so .d " ; a .aadas rcqiq iFT,oLorrii.;.;j.,. _..,.".." ",."."
*,..Js"y_..%,.-.j... ?;l,ft;;
il#-i.rif lffilfl,li"rYiiil!.#. tri*L.,lliu,it?1tr3it;*r';t*-1?rtritii:lifi:*3;l*!|;:t"fJJa,"#j[f]m**"i,,*m*tf,n"*rl.*imee,tre o,hsdm,ns,,s uirarraian ft;J;;;t;i;$0@6,he,
--r,"'.]ri.?Jrrr r.' ],i;Li,i#,!; t.ti? g!#Tgj N.fi::!. ?^r".: : :1,,,,',.,,'
Sample Measurement
Acid dagestion by suitable aciddepended on different samplematerial (as below table)
Microwave digestion with
HNO3/HCVHFAdd appropri€te amount ofdige6tion reagent
Heat to appropriate
temperature to extract
Cool, filter digestate
through filter
Add diphenyl-carbazide for
color development
measure the absorbanceat 540 nm by UV-VIS
Test ReportEPISIL TECHNOLOGIES INC.NO. 3, INNOVATION ROAD 1,
Page: 4 of4
|ltI |||| ll |lllc.
No.. CE12012J12342 Da['e :2OiZOr1a
SCIENCE BASED INDUSTRIAL PARK, HSINCHU, TAIWAN, R. O.
t The togted sample / part is marked by an afiow if il,s shown on the photo. ,
*' End of Report ".
i3fi:fi'rTiT:,jlT'f:f:):a}jij1if,1ii;i]Epf1,igg]l]f:hj.:-1,ej.J'|j:'g]lii1E1{.?M€mdbqd"edeii"i{iFl;ii',;#i:ilit"-.iPj":"1";:i{*l **{'.i;""::;r#;t#H.*f;3 ';:"'.r.",i":;Tasi;:"irirr.i"";;ts
'.'dr- ha , " d L . 's :"a;""":ii:.""::{e r:i::.:: iiiJ:T;" jT;:q T.: ;;':;"-*.fl'":,:,i ":.;g;i}e#;i"f**i.?,131;:i:;i;'"".,:;;JJi:,i.:3e,i:i"J":f:."";.,;ri"";$;r;;,.;aL;,.,;:i"{1r."}",,e:,:i;j;."tg"t,lr';:,.ii"iT^L::. ++, ,,r.,",r r;l,i.ti,.ii.|.il,i!,,1!l;1u;;*.|*i,,T1:1:,... " , : l_:*
.__ _
L2342
Test Report Number : TWNC00253298
Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited
K. Y. Liang Director
This report shall not be reproduced except in full, without the written approval of the laboratory.
Page 1 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Applicant: Littelfuse Philippines Inc. Date : Apr 25, 2012 LIMA Technology Center, Lipa City,
Malvar, Batangas
Sample Description:
One (1) group of submitted samples said to be : Sample Description : UDFN (SP3000 series product) Date Sample Received : Apr 17, 2012 Date Test Started : Apr 18, 2012
Test Conducted:
As requested by the applicant, for details please refer to attached pages.
Number : TWNC00253298 Test Conducted
Page 2 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
(Ⅰ) Test Result Summary: Result (ppm)
Test Item Black Electronic Component (Mixed
All Parts)
Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ND Dibutyl Phthalate (DBP) ND Benzyl Butyl Phthalate (BBP) ND
Others Hexabromocyclododecane (HBCDD) ND
Remarks : ppm = Parts per million based on weight of tested sample ND = Not detected
Responsibility of Chemist: Irene Chiou / Cathy Chen
Date Sample Received : Apr 17, 2012 Test Period : Apr 18, 2012 To Apr 19, 2012
(Ⅱ) Test Method:
Test Item Test method Reporting Limit
Phthalates With reference to EN 14372: 2004, bysolvent extraction and determined byGC-MS.
50 ppm
Hexabromocyclododecane(HBCDD)
With reference to USEPA 3540C, by solvent extraction and determined byGC-MSD
10 ppm
Remark : Reporting Limit = Quantitation limit of analyte in sample
Number : TWNC00253298 Test Conducted
Page 3 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
(Ⅲ) Measurement Flowchart: Test For Phthalates Contents Reference Method: EN 14372: 2004
Sampling/grinding or cutting
Weigh sample and add organic solvent
By solvent extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
Number : TWNC00253298 Test Conducted
Page 4 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
(Ⅲ) Measurement Flowchart: Test For Hexabromocyclododecane (HBCDD) Reference Standard：USEPA 3540C
End of Report
Sampling/grinding or cutting
Weigh sample and add organic solvent
By soxhlet extraction
Concentrate the extract and make up with organic solvent
Analyzed by GC-MSD
Number : TWNC00253298 Test Conducted
Page 5 of 5 Intertek Testing Services Taiwan Ltd.
8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓
Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401
Photo
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