Food Compendium 2013 Volume

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    COMPENDIUM OFINTERNATIONAL METHODS

    OF WINE AND MUST ANALYSIS

    INTERNATIONAL ORGANISATION

    OF VINE AND WINE

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    INTERNATIONAL ORGANISATION OF VINE AND WINE

    COMPENDIUMOF INTERNATIONAL

    METHODS OF WINE

    AND MUST ANALYSIS

    EDITION 2013 VOLUME1

    I NCLUDED :

    Resolutions adopted in I zmir (Turkey)

    10thA.G.22 June 2012

    OIV-18,RUE DAGUESSEAU -75008PARIS

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    Printed in Paris (France)

    18, rue dAguesseau

    75008 Paris, France

    Legal Deposit : February 2013

    ISBN : 979-10-91799-06-5

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    COMPENDIUM OF INTERNATIONAL METHODS OF ANALYSIS-OIV

    Table of contents

    OIV-MA-INT-00-2013 1

    General organization of the Compendium

    Table of contents

    Foreword

    ANNEX A METHODS OF ANALYSIS OF WINES AND MUSTS

    SECTION 1 DEFINITIONS AND GENERAL PRINCIPLES

    SECTION 2 PHYSICAL ANALYSIS

    SECTION 3 CHIMICAL ANALYSIS

    SECTION 3.1 ORGANIC COMPOUNDS

    SECTION 3.1.1 SUGARS

    SECTION 3.1.2 ALCOHOLS

    SECTION 3.1.3 ACIDS

    SECTION 3.1.4 GASSECTION 3.1.5 OTHER ORGANIC COMPOUNDS

    SECTION 3.2 NON ORGANIC COMPOUNDS

    SECTION 3.2.1 ANIONS

    SECTION 3.2.2 CATIONS

    SECTION 3.2.3 OTHER NON ORGANIC COMPOUNDS

    SECTION 4 MICROBIOLOGICAL ANALYSIS

    SECTION 5 OTHER ANALYSIS

    ANNEX B - CERTIFICATES OF ANALYSIS

    ANNEX C - MAXIMUM ACCEPTABLE LIMITS OF VARIOUS SUBSTANCES

    ANNEX D ADVICES

    ANNEX E LABORATORY QUALITY ASSURANCE

    ANNEX F SPECIFIC METHODS FOR THE ANALYSIS OF GRAPE SUGAR(RECTIFIED CONCENTRATED MUSTS)

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    COMPENDIUM OF INTERNATIONAL METHODS OF ANALYSIS-OIV

    Table of contents

    OIV-MA-INT-00-2013 3

    SECTION 3 CHIMICAL ANALYSIS

    SECTION 3.1 ORGANIC COMPOUNDS

    SECTION 3.1.1 SUGARS

    - Reducing substances (A 4 revised by 377/2009) OIV-MA-AS311-01A IV

    - Reducing sugars (clarification) (type IV) OIV-MA-AS311-01B Withdrawn- Reducing sugars (titrimtrie) (type II) OIV-MA-AS311-01C Withdrawn

    - Glucose and fructose (enzymatic method) (revised by

    377/2009)OIV-MA-AS311-02 II

    - Dosage of sugars by HPLC (Oeno 23/2003) OIV-MA-AS311-03 II

    - Stabilisation of musts to detect Addition of sucrose (A 5) OIV-MA-AS311-04

    - Determination of the deuterium distribution in ethanol

    derived from fermentation of grape musts, concentrated

    grape musts, rectified concentrated grape musts and wines

    by application of nuclear magnetic resonance (SNIFNMR/

    RMNFINS) ( Oeno 426-2011)

    OIV-MA-AS311-05 II

    - Polyols derived from sugars (Oeno 9/2006) OIV-MA-AS311-06 IV

    - Glucose and fructose (pHmetry) (Oeno 10/2006 revised by

    377/2009)OIV-MA-AS311-07 III

    - Glucose, fructose and saccharose (pHmetry) (Oeno11/2006 revised by 377/2009)

    OIV-MA-AS311-08 IV

    SECTION 3.1.2 ALCOHOLS

    - Alcoholic strength by volume (pycnometry, frequency

    oscillator, hydrostatic balance) (A2; 8/2000; 24/2003;

    revised by 377/2009)

    OIV-MA-AS312-01A I

    - Alcoholic strength by volume (hydrometer,refractometry) (A2 revised by 377/2009)

    OIV-MA-AS312-01B IV

    - Tables of correction (A2) OIV-MA-AS312-02

    - Methanol (GC) (A 41 revised by 377/2009) OIV-MA-AS312-03A IV

    - Methanol (colorimetry) (A 41 revised by 377/2009) OIV-MA-AS312-03B IV

    - Glycerol and 2,3- butanediol (A 21 revised by 377/2009) OIV-MA-AS312-04 IV

    - Glycerol (enzymatic method) (Recueil OIV ed. 1990revised by 377/2009)

    OIV-MA-AS312-05 IV

    -Determination of isotopic ratio of ethanol (Oeno 17/2001) OIV-MA-AS312-06 II

    - Glycerol (GC-C-IRMS or HPLC-IRMS method) (OIV-

    Oeno 343-2010)OIV-MA-AS312-07 IV

    SECTION 3.1.3 ACIDS

    - Total Acidity (A 10 revised by 377/2009) OIV-MA-AS313-01 I

    - Volatile Acidity (A 11 revised by 377/2009) OIV-MA-AS313-02 I

    - Fixed Acidity (A 11 revised by 377/2009) OIV-MA-AS313-03 I

    - Organic Acids : HPLC (Recueil OIV ed. 1990 revised by

    377/2009)OIV-MA-AS313-04 IV

    - Tartaric Acid (gravimetry) (A 12 revised by 377/2009) OIV-MA-AS313-05A IV- Tartaric Acid (colorimetry) (A 12) OIV-MA-AS313-05B Withdrawn

    http://../Compendium%202013%20doc/MA-E-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-E-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-E-AS311-03-SUCRES.dochttp://../Compendium%202013%20doc/MA-E-AS311-03-SUCRES.dochttp://../Compendium%202013%20doc/MA-E-AS311-03-SUCRES.dochttp://../Compendium%202013%20doc/MA-E-AS311-03-SUCRES.dochttp://../Compendium%202013%20doc/MA-E-AS311-04-STAMOU.dochttp://../Compendium%202013%20doc/MA-E-AS311-04-STAMOU.dochttp://../Compendium%202013%20doc/MA-E-AS311-05-ENRRMN.dochttp://../Compendium%202013%20doc/MA-E-AS311-05-ENRRMN.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-E-AS312-02-TALVOL.dochttp://../Compendium%202013%20doc/MA-E-AS312-03-METHAN.dochttp://../Compendium%202013%20doc/MA-E-AS312-03-METHAN.dochttp://../Compendium%202013%20doc/MA-E-AS312-03-METHAN.dochttp://../Compendium%202013%20doc/MA-E-AS312-03-METHAN.dochttp://../Compendium%202013%20doc/MA-E-AS312-04-GLYBUT.dochttp://../Compendium%202013%20doc/MA-E-AS312-04-GLYBUT.dochttp://../Compendium%202013%20doc/MA-E-AS312-04-GLYBUT.dochttp://../Compendium%202013%20doc/MA-E-AS312-04-GLYBUT.dochttp://../Compendium%202013%20doc/MA-E-AS312-05-GLYENZ.dochttp://../Compendium%202013%20doc/MA-E-AS312-05-GLYENZ.dochttp://../Compendium%202013%20doc/MA-E-AS312-05-GLYENZ.dochttp://../Compendium%202013%20doc/MA-E-AS312-06-ETHANO.dochttp://../Compendium%202013%20doc/MA-E-AS312-06-ETHANO.dochttp://../Compendium%202013%20doc/MA-E-AS313-01-ACITOT.dochttp://../Compendium%202013%20doc/MA-E-AS313-01-ACITOT.dochttp://../Compendium%202013%20doc/MA-E-AS313-01-ACITOT.dochttp://../Compendium%202013%20doc/MA-E-AS313-01-ACITOT.dochttp://../Compendium%202013%20doc/MA-E-AS313-01-ACITOT.dochttp://../Compendium%202013%20doc/MA-E-AS313-01-ACITOT.dochttp://../Compendium%202013%20doc/MA-E-AS312-06-ETHANO.dochttp://../Compendium%202013%20doc/MA-E-AS312-06-ETHANO.dochttp://../Compendium%202013%20doc/MA-E-AS312-05-GLYENZ.dochttp://../Compendium%202013%20doc/MA-E-AS312-05-GLYENZ.dochttp://../Compendium%202013%20doc/MA-E-AS312-04-GLYBUT.dochttp://../Compendium%202013%20doc/MA-E-AS312-04-GLYBUT.dochttp://../Compendium%202013%20doc/MA-E-AS312-03-METHAN.dochttp://../Compendium%202013%20doc/MA-E-AS312-03-METHAN.dochttp://../Compendium%202013%20doc/MA-E-AS312-02-TALVOL.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-F-AS311-02-GLUFRU.dochttp://../Compendium%202013%20doc/MA-E-AS311-05-ENRRMN.dochttp://../Compendium%202013%20doc/MA-E-AS311-04-STAMOU.dochttp://../Compendium%202013%20doc/MA-E-AS311-03-SUCRES.dochttp://../Compendium%202013%20doc/MA-E-AS311-03-SUCRES.dochttp://../Compendium%202013%20doc/MA-E-AS311-02-GLUFRU.doc
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    COMPENDIUM OF INTERNATIONAL METHODS OF ANALYSIS-OIV

    Table of contents

    OIV-MA-INT-00-2013 4

    - Lactic Acid - chemical method (A 27) OIV-MA-AS313-06 Withdrawn

    - Lactic Acid - enzymatic method (Recueil OIV ed. 1990

    revised by 377/2009)OIV-MA-AS313-07 II

    - Citric Acid - chemical method (A 29) OIV-MA-AS313-08 IV

    - Citric Acid - enzymatic method (Recueil OIV ed. 1990revised by 377/2009)

    OIV-MA-AS313-09 II

    - Total malic Acid: usual method (A 33 revised by

    377/2009) OIV-MA-AS313-10 IV

    - L-malic Acid: enzymatic method (Recueil OIV ed. 1990

    revised by 377/2009)OIV-MA-AS313-11 II

    - D-malic Acid: enzymatic method (Oeno 6/98 revised by

    377/2009)OIV-MA-AS313-12A II

    - D-malic Acid: enzymatic method low concentrations

    (Oeno 16/2002 revised by 377/2009)OIV-MA-AS313-12B IV

    - L-ascorbic Acid (spectrofluorimetry) (A 28 revised by

    377/2009)OIV-MA-AS313-13A IV

    - L-ascorbic Acid (spectrophotometry) (A 28) OIV-MA-AS313-13B Withdrawn

    - Sorbic Acid (spectrophotometry) (A 30 revised by377/2009)

    OIV-MA-AS313-14A IV

    - Sorbic Acid (GC ) (A 30 revised by 377/2009) OIV-MA-AS313-14B IV

    - Sorbic Acid (TLC) (A 30 revised by 377/2009) OIV-MA-AS313-14C IV- pH (A31 revised by Oeno 438-2011) OIV-MA-AS313-15 I

    - Organic acid : ionic chromatography (Oeno 23/2004) OIV-MA-AS313-16 IV

    - Shikimic acid (Oeno 33/2004) OIV-MA-AS313-17 II

    - Sorbic acid (capillary electrophoresis) (Oeno 4/2006) OIV-MA-AS313-18 IV

    - Organic acids and sulphates (capillary electrophoresis)

    (Oeno 5/2006, extended by Oeno 407-2011)OIV-MA-AS313-19

    II

    III- Sorbic, benzoic, salicylic acids (Oeno 6/2006) OIV-MA-AS313-20 IV

    - Metatartaric acid (Oeno 10/2007) OIV-MA-AS313-21 IV

    - Determination of L-ascorbic acid and D-iso-ascorbic acidby HPLC (Oeno 11/2008)

    OIV-MA-AS313-22 II

    - Identification of L- tartaric acid (Oeno 12/2008) OIV-MA-AS313-23 IV

    SECTION 3.1.4 GAS

    - Carbone Dioxide (A 39 modified by oeno 21/2003 and

    completed by Oeno 3/2006 revised by 377/2009)OIV-MA-AS314-01 II

    - Overpressure measurment of sparkling wines (Oeno

    21/2003)OIV-MA-AS314-02 I

    - Determination of the carbon isotope ratio13