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Diffusion Vacuum Pumpby Random_Canadian on April 15, 2012

Table of Contents

Diffusion Vacuum Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Intro:   Diffusion Vacuum Pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Step 1:   Materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Step 2:   Lower end . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Step 3:   Vacuum port and braze together . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Step 4:   The active cones! . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Step 5:   Silicone oil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Step 6:   Finish the top . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Step 7:   Test the pump . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Related Instructables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

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Author:Random_CanadianI seem to keep breaking things....

Intro:  Diffusion Vacuum PumpPlease look up the definition of a Diffusion Vacuum Pump before continuing!

This pump is made from readily available materials and has been shown to achieve a .022 TORR vacuum!!!!

Use extreme caution when working with vacuum

This pump needs a "Roughing" pump to get down to a near vacuum then it will work as described.No a refrigerator compressor will not work as a "Roughing" Pump for thisNo a vacuum cleaner will not work either!

You will need a refrigeration service type pump for the "Roughing" of the vacuum.

Yes you may have to go to IKEA to get some of the parts!

Step 1: MaterialsYou will need a stainless steel tube (I used an exhaust pipe section)Some 1/4 inch copper tube andstainless steel flat sections.

I found that the local scrap yard had lots of stainless steel parts. Selecting the right few took a couple of trips.

You will also need to know how to braze. I used stainless brazing rod for joining all parts.

I used a stainless 2.75 od exhaust pipe adapter for the body. Some scrap stainless flats for the ends.

All cutting was done with a Dremel and cut-off abrasive wheel.

Several Ikea stainless cups were sacrificed for this build!

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Step 2: Lower endThe base was a scrap cut stainless round. the edged were smoothed and a 10x32 nut was brazed in the center.This was then brazed to the center of the exhaust pipe.

a 1/2 inch hole was drilled into the exhaust pipe for a vacuum port. This was about 1 inch from the bottom edge.

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Step 3: Vacuum port and braze togetherAdd a vacuum port that is at lease 1/2 inch in diameter and up and away from the body of the pump.

I used a 1/2 inch tube cut an brazed together at a 45 degree point then brazed tot he body of the pump.

It is important to make sure that there is no leaks!!!

I tested this by blocking the vacuum port then inverting the pump body and drawing a deep vacuum on my vacuum table. I got down to 150 microns which was a reallygood indication that there were no leaks.

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Step 4: The active cones!I used some Ikea stainless glasses and dollar store spice jars for the internal cone structure.

All were cut, drilled and welded as in the photos.

The spice jars were cut off and brazed together.

The ikea glasses were drilled and cut as shown in the pics.

All cone assemblies were to fit inside of the the outer exhaust tube. No parts were to extend outside of the tube.

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Step 5: Silicone oilGetting the oil for proper pump operation is actually quite simple..

It can be refined from spray lube or harvested from a photocopier (fuser oil)

It can be purchased.

Silicone oil is expensive but seems to be the oil of choice for these pumps.

It is non-flammable and non-reactive. Plus is works great!

I harvested fro a spray lube by first spraying the entire contents into a jar. I heated and vacuumed the jar until I had pure silicone oil. It took quite a while and i did gothrough quite a bit of vacuum pump oil but the end oil works great!. Do not heat it in atmosphere as it will burn and not work properly in the future!

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Step 6: Finish the topI used a section of stainless steel for the top.

The opening was marked then perimeter drilled then cut and finished with a Dremel and a half round file.

The opening had to have the same inner diameter as the the exhaust pipe.

All slag from the brazing was then cleaned off with a wire brush.

The end plate was then brazed to the top of the pump assemble.

I brazed 2 opposite sides than all the way around the edge to make a complete seal.

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Step 7: Test the pumpI used a jam jar with a silicone baking mat to test the final seal.

The inner cones were bolted into place then the oil was added. The assembly was placed into a shop vise and I used a propane torch to heat the bottom of the pump. Inthe future a stove element will be used but this was just a test..

I attached the pump to the vacuum port then ran the pump for about a 1/2 hour. I was able to get a vacuum of around 130 microns.

With no water cooling and constant heating got the vacuum down to less than 22 microns. This is far deeper than my refrigeration pump has ever gone!!! I need to watercool the pump body to get some extreme vacuums!

That is 0.022 TORR .. Let the games begin!

I will be making extensive use of this pump in the near future for some amazing instructables!

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