1l 1H NMR (400 MHz, CDCl3 · 1l. 13. C NMR (100 MHz, CDCl. 3) HN S O O I S. Electronic Supplementary Material (ESI) for Chemical Communications This journal is © The Royal Society

1l 1H NMR (400 MHz, CDCl3)

HNS

O

O

I

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

ManojitP

Text Box

Copies of 1H and 13C NMR

1l 13C NMR (100 MHz, CDCl3)

HNS

O

O

I

S


Copies of 1H and 13C NMR

3a 1H NMR (400 MHz, CDCl3)

NN

I

CH3

Ts


3a 13C NMR (100 MHz, CDCl3)

NN

I

CH3

Ts


3b 1H NMR (400 MHz, CDCl3)

NN

I

F

Ms


3b 13C NMR (100 MHz, CDCl3)

NN

I

F

Ms


3c 1H NMR (400 MHz, CDCl3)

NN

I

Cl

Ms


3c 13C NMR (100 MHz, CDCl3)

NN

I

Cl

Ms


3d 1H NMR (400 MHz, CDCl3)


3d 13C NMR (100 MHz, CDCl3)


3e 1H NMR (400 MHz, CDCl3)

NN

I

F

Ts


3e 13C NMR (100 MHz, CDCl3)


3f 1H NMR (400 MHz, CDCl3)


3f 13C NMR (100 MHz, CDCl3)


3g 1H NMR (400 MHz, CDCl3)

NN

I

Cl

Ts


3g 13C NMR (100 MHz, CDCl3)

NN

I

Cl

Ts


3h 1H NMR (400 MHz, CDCl3)


3h 13C NMR (100 MHz, CDCl3)


3i 1H NMR (400 MHz, CDCl3)

NN

I

CH3

S OO

S


3i 13C NMR (100 MHz, CDCl3)

NN

I

CH3

S OO

S


3j 1H NMR (400 MHz, CDCl3)

NN

I

S OO

S

F


3j 13C NMR (100 MHz, CDCl3)

NN

I

S OO

S

F


3k 1H NMR (400 MHz, CDCl3)

NN

I

S OO

S


3k 13C NMR (100 MHz, CDCl3)

NN

I

S OO

S



NN

I

CH3

Ms



NN

I

CH3

Ms


3m 1H NMR (400 MHz, CDCl3)


3m 13C NMR (100 MHz, CDCl3)

NN

I

F

Ms


3n 1H NMR (400 MHz, CDCl3)


3n 13C NMR (100 MHz, CDCl3)


3o 1H NMR (400 MHz, CDCl3)


3o 13C NMR (100 MHz, CDCl3)

NN

I

Me

Ts


3p 1H NMR (400 MHz, CDCl3)


3p 13C NMR (100 MHz, CDCl3)

NN

I

F

Ts


3q 1H NMR (400 MHz, CDCl3)

NN

I

Cl

Ts


3q 13C NMR (100 MHz, CDCl3)


3r 1H NMR (400 MHz, CDCl3)

NN

I

Br

Ts


3r 13C NMR (100 MHz, CDCl3)

NN

I

Br

Ts


3s 1H NMR (400 MHz, CDCl3)


3s 13C NMR (100 MHz, CDCl3)

NBn

N

I

Ts

F


3t 1H NMR (400 MHz, CDCl3)

N NN

I

F

Ts

Cl


3t 13C NMR (100 MHz, CDCl3)

N NN

I

F

Ts

Cl


3u 1H NMR (400 MHz, CDCl3)


3u 13C NMR (100 MHz, CDCl3)


3v1H NMR (400 MHz, CDCl3)

NN

O2N

S OO

I

F

S


3v 13C NMR (100 MHz, CDCl3)

NN

O2N

S OO

I

F

S


3w 1H NMR (400 MHz, CDCl3)

NN

S OO

Br


3w 13C NMR (100 MHz, CDCl3)

NN

S OO

Br


4a 1H NMR (400 MHz, CDCl3)


4a 13C NMR (100 MHz, CDCl3)


4b 1H NMR (400 MHz, CDCl3)


4b 13C NMR (100 MHz, CDCl3)



NN

Ms

Cl



NN

Ms

Cl


4d 1H NMR (400 MHz, CDCl3)

NN

Ms


4d 13C NMR (100 MHz, CDCl3)

NN

Ms


4e 1H NMR (400 MHz, CDCl3)

NN

Ts

F


4e 13C NMR (100 MHz, CDCl3)

NN

Ts

F


4f 1H NMR (400 MHz, CDCl3)

NN

Ts


4f 13C NMR (100 MHz, CDCl3)

NN

Ts


4g 1H NMR (400 MHz, CDCl3)


4g 13C NMR (100 MHz, CDCl3)


4h 1H NMR (400 MHz, CDCl3)

NN

Ts

Br


4h 13C NMR (100 MHz, CDCl3)

NN

Ts

Br


4i 1H NMR (400 MHz, CDCl3)


4i 13C NMR (100 MHz, CDCl3)


4j 1H NMR (400 MHz, CDCl3)

NN

S OO

S

F


4j 13C NMR (100 MHz, CDCl3)

NN

S OO

S

F


4k 1H NMR (400 MHz, CDCl3)

NN

S OO

S


4k 13C NMR (100 MHz, CDCl3)



N NMs

CH3



N NMs

CH3


4m 1H NMR (400 MHz, CDCl3)


4m 13C NMR (100 MHz, CDCl3)


4n 1H NMR (400 MHz, CDCl3)


4n 13C NMR (100 MHz, CDCl3)


4o 1H NMR (400 MHz, CDCl3)


4o 13C NMR (100 MHz, CDCl3)

N NTs


4p 1H NMR (400 MHz, CDCl3)


4p 13C NMR (100 MHz, CDCl3)


4q 1H NMR (400 MHz, CDCl3)


4q 13C NMR (100 MHz, CDCl3)

N NTs

Cl


4r 1H NMR (400 MHz, CDCl3)


4r 13C NMR (100 MHz, CDCl3)


4s 1H NMR (400 MHz, CDCl3)


4s 13C NMR (100 MHz, CDCl3)

NN

Ts

F


4t 1H NMR (400 MHz, CDCl3)

N NN

Ts

F

Cl


4t 13C NMR (100 MHz, CDCl3)

N NN

Ts

F

Cl


4u 1H NMR (400 MHz, CDCl3)

N

MeO

NS O

O

S


4u 13C NMR (100 MHz, CDCl3)

N

MeO

NS O

O

S


4v 1H NMR (400 MHz, CDCl3)

N

O2N

N

F

S OO

S


4v 13C NMR (100 MHz, CDCl3)


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1l 1H NMR (400 MHz, CDCl3 · 1l. 13. C NMR (100 MHz, CDCl. 3) HN S O O I S. Electronic Supplementary Material (ESI) for Chemical Communications This journal is © The Royal Society